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  • P-ISSN 1225-0163
  • E-ISSN 2288-8985

Isolation and Gas Chromatographic Analysis of Lupenone and Lupeol from Sorbus Cortex

Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
1999, v.12 no.2, pp.136-140
Lee, Sang-Myoung
Lee, Cheal-Gyu
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Abstract

Lupenone and lupeol, the triterpenoids of Sorbus Cortex, were isolated with silica gel column chromatography and used as the standard substances for the quantitative analysis. The compounds were identified with IR, NMR, EI-MS. They were separated on VA-5MS [(5%-phenyl)methylpolysiloxane, <TEX>$30m{\times}0.25mm$</TEX>, <TEX>$0.25{\mu}m$</TEX>] column by gas-chromatograph. The contents of lupeone and lupeol in three different samples of Sorbus Cortex were in the range of 0.050~0.056% and 0.772~0.834%, respectively.

keywords
sorbus cortex, Sorbus commixta, Sorbus amurensis, lupenone, lupeol


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