- P-ISSN 1225-0163
- E-ISSN 2288-8985
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- P-ISSN1225-0163
- E-ISSN2288-8985
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Preparation and characterization of fullerene dimer [C120] by trichloroperbenzoic acid oxidation method
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2007, v.20 no.2, pp.124-130
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(2007). Preparation and characterization of fullerene dimer [C120] by trichloroperbenzoic acid oxidation method. Analytical Science and Technology, 20(2), 124-130.
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Abstract
In this study, we present the preparation and characterization of oxidized fullerene and fullerene dimer [<TEX>$C_{120}$</TEX>]. From the XRD data, other weak peaks with pristine fullerene [<TEX>$C_{60}$</TEX>] peaks were observed in the X-ray diffraction patterns for fullerene dimer [<TEX>$C_{120}$</TEX>]. SEM micrographs for the fullerene dimer [<TEX>$C_{120}$</TEX>] indicated that practically all the surface state was shown the drastic morphology changes and its outer surface is clearly visible and resulted in clogging and frost-like formation. From the MALDI-TOF mass spectra, the differences in the spectra recorded on two kinds of fullerene are due to the oxidation including chemical bonding and bridging between the <TEX>$C_{60}$</TEX> molecules. We also obtained additional information from FT-IR spectra on functional component on the chemically modified surface of oxidized fullerene and fullerene dimer [<TEX>$C_{120}$</TEX>].
- keywords
- fullerene dimer [<TEX>$C_{120}$</TEX>], XRD, SEM, MALDI-TOF, FT-IR
Reference
1
G. Cao, (2004) Nanostructures and nanomaterials, Imperialcollege press
2
R. Setton, (1998) Carbon molecules and materials, Taylor & Francis
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