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Measurement of 1,4-dioxane in surface water by headspace GC-MS
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2014, v.27 no.1, pp.22-26
https://doi.org/10.5806/AST.2014.27.1.22
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(2014). Measurement of 1,4-dioxane in surface water by headspace GC-MS. Analytical Science and Technology, 27(1), 22-26, https://doi.org/10.5806/AST.2014.27.1.22
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Abstract
1,4-Dioxane was classified as a Group 2B carcinogen by the International Agency for Research onCancer. The compound was measured in surface water with a headspace gas chromatographic mass spectrometricdetection. A 5 mL water sample was placed in a 10 mL headspace vial and saturated with NaCl, and thesolution was spiked with 1,4-dioxane-d8 as an internal standard and sealed with a cap. Water samples werecollected from twenty-two basins of Gum-River on June and September 2012, respectively. As a result, 1,4-dioxane was detected in the concentration range of 0.49-43.0 μg/L (mean 2.0 μg/L) in the frequency of about30% in surface water samples.
- keywords
- 1, 4-Dioxane, surface water, headspace extraction, gas chromatography-mass spectrometry
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