- P-ISSN 1225-0163
- E-ISSN 2288-8985
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- P-ISSN1225-0163
- E-ISSN2288-8985
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Synthesis, crystal structure, and analytical characterizations of amphiphilic palladium(II) compound containing bis(benzylthio)methylenepropanedioate
분석과학 / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2023, v.36 no.4, pp.198-203
https://doi.org/10.5806/AST.2023.36.4.198
(Department of Chemistry Education and Institute of Fusion Science, Jeonbuk National University)
Tae,
H.
N.
(2023). . 분석과학, 36(4), 198-203, https://doi.org/10.5806/AST.2023.36.4.198
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Abstract
The reaction of cis-protected (Me4en)Pd(II) species with potentially multidentate bis(benzylthio)methylenepropanedioate (L) was carried out to obtain a monometallic compound, [(Me4en)Pd(L)], in O,O’-coordination mode. The bis(benzylthio)methylene group was bent strikingly from the palladium square plane at the dihedral angle of 70.40°. The physicochemical properties of the present palladium(II) compound were fully characterized by means of infrared and nuclear magnetic resonance spectroscopy, thermogravimetric analysis, and single-crystal X-ray diffraction measurement.
- keywords
- coordination mode, crystal engineering, X-ray diffraction, NMR spectroscopy
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