ACOMS+ 및 학술지 리포지터리 설명회

  • 한국과학기술정보연구원(KISTI) 서울분원 대회의실(별관 3층)
  • 2024년 07월 03일(수) 13:30
 

  • P-ISSN2233-4203
  • E-ISSN2093-8950
  • ESCI, SCOPUS, KCI

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  • P-ISSN 2233-4203
  • E-ISSN 2093-8950

Simple and Direct Quantitative Analysis for Quinidine Drug in Fish Tissues

Mass Spectrometry Letters / Mass Spectrometry Letters, (P)2233-4203; (E)2093-8950
2017, v.8 no.1, pp.8-13
https://doi.org/10.5478/MSL.2017.8.1.8
Yuan-Chin Chen (National Sun Yat-Sen University)
Hani Nasser Abdelhamid (Assuit University)
Hui-Fen Wu (National Sun Yat-Sen University)
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Abstract

Analysis of quinidine for fish tissues using single drop microextraction (SDME) coupled with atmospheric pressure matrix assisted laser desorption/ionization mass spectrometry (AP-MALDI-MS) are reported. Optimization conditions; such as extraction solvent, extraction time, pH of the aqueous solution, salt additions (NaCl), stirring rate, matrix type and concentration are investigated. Linear dynamic range (μM), limit of detection, relative recovery%, and enrichment factor are 0.08-9.2, 0.05, 94.8±3.1- 98.5±3.3%, 4.34±0.28-4.40±0.30, respectively. SDME-AP-MALDI-MS shows good intraday and interday reproducibility.

keywords
quinidine, fish tissues, environmental analysis, quantitative analysis, extraction, SDME-AP-MALDI-MS


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투고일Submission Date
2016-11-24
수정일Revised Date
2017-01-02
게재확정일Accepted Date
2017-02-02
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