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- E-ISSN 2093-8950
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- P-ISSN2233-4203
- E-ISSN2093-8950
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Simple and Direct Quantitative Analysis for Quinidine Drug in Fish Tissues
Mass Spectrometry Letters / Mass Spectrometry Letters, (P)2233-4203; (E)2093-8950
2017, v.8 no.1, pp.8-13
https://doi.org/10.5478/MSL.2017.8.1.8
(National Sun Yat-Sen University)
(Assuit University)
(National Sun Yat-Sen University)
(Assuit University)
(National Sun Yat-Sen University)
Chen,
Y.,
Abdelhamid,
H. N.,
&
Wu,
H.
(2017). . Mass Spectrometry Letters, 8(1), 8-13, https://doi.org/10.5478/MSL.2017.8.1.8
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Abstract
Analysis of quinidine for fish tissues using single drop microextraction (SDME) coupled with atmospheric pressure matrix assisted laser desorption/ionization mass spectrometry (AP-MALDI-MS) are reported. Optimization conditions; such as extraction solvent, extraction time, pH of the aqueous solution, salt additions (NaCl), stirring rate, matrix type and concentration are investigated. Linear dynamic range (μM), limit of detection, relative recovery%, and enrichment factor are 0.08-9.2, 0.05, 94.8±3.1- 98.5±3.3%, 4.34±0.28-4.40±0.30, respectively. SDME-AP-MALDI-MS shows good intraday and interday reproducibility.
- keywords
- quinidine, fish tissues, environmental analysis, quantitative analysis, extraction, SDME-AP-MALDI-MS
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- 투고일Submission Date
- 2016-11-24
- 수정일Revised Date
- 2017-01-02
- 게재확정일Accepted Date
- 2017-02-02
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