- P-ISSN 2233-4203
- E-ISSN 2093-8950
- 권한신청
- P-ISSN2233-4203
- E-ISSN2093-8950
- ESCI, SCOPUS, KCI
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Determination of Emamectin Benzoate in Eel, Halibut, and Shrimp Using QuEChERS-EDTA and LC-MRM
Mass Spectrometry Letters / Mass Spectrometry Letters, (P)2233-4203; (E)2093-8950
2018, v.9 no.4, pp.100-104
https://doi.org/10.5478/MSL.2018.9.4.100
(Dankook University)
(Dankook University)
(Dankook University)
(Chung-Ang University)
(Konkuk University)
(Dankook University)
(Dankook University)
(Dankook University)
(Chung-Ang University)
(Konkuk University)
(Dankook University)
Cho,
H. R.,
Kim,
D. Y.,
Lee,
H. C.,
한상범,
Shin,
H.,
&
Choi,
Y.
S.
(2018). . Mass Spectrometry Letters, 9(4), 100-104, https://doi.org/10.5478/MSL.2018.9.4.100
- 다운로드 수
- 조회수
Abstract
As a part of efforts to establish the positive list system (PLS) in South Korea, a method to determine residual ema- mectin benzoate (EB) in various aquatic products using QuEChERS-EDTA and LC-MRM was developed. The developed method was validated in the aspects of specificity, linearity (correlation coefficient of at least 0.996), sensitivity (the limit of detection and the lower limit of quantitation ≤ 5 ng/g), recovery (the recovery range of 87.4 and 96.2), and precision (the relative standard deviation of recovery between 0.9 and 13.5). Additionally, the validated method was successfully applied for monitor- ing EB contamination in eel, halibut, and shrimp collected from local food markets. To our knowledge, the present method is the first one to determine residual EB in various aquatic products at the level satisfying the PLS and could contribute to the estab- lishment of the PLS in South Korea.
- keywords
- Emamectin, Aquatic products, QuEChERS, EDTA, MRM, PLS
참고문헌
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- 투고일Submission Date
- 2018-12-08
- 수정일Revised Date
- 2018-12-13
- 게재확정일Accepted Date
- 2018-12-13
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