Development of a Chloroform Reference Material for the Proficiency Testing of Hazardous Compounds in Commercial Consumer Chemical Products Under the Consumer Chemical Products and Biocide Safety Management Act (K-BPR)

Lee Sang Tak; Lee Jae-ung; Kim Joo-Hyon; Oh Han Bin

doi:10.5478/MSL.2019.10.4.112

P-ISSN2233-4203
E-ISSN2093-8950
ESCI, SCOPUS, KCI

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P-ISSN 2233-4203
E-ISSN 2093-8950

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Vol.10, No.4

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Development of a Chloroform Reference Material for the Proficiency Testing of Hazardous Compounds in Commercial Consumer Chemical Products Under the Consumer Chemical Products and Biocide Safety Management Act (K-BPR)

Mass Spectrometry Letters / Mass Spectrometry Letters, (P)2233-4203; (E)2093-8950

2019, v.10 no.4, pp.112-116

https://doi.org/10.5478/MSL.2019.10.4.112

Lee Sang Tak (Sogang University)
Lee Jae-ung (Sogang University)
Kim Joo-Hyon (National Institute of Environmental Research)
Oh Han Bin (Sogang University)

Lee, S. T., Lee, J., Kim, J., & Oh, H. B. (2019). Development of a Chloroform Reference Material for the Proficiency Testing of Hazardous Compounds in Commercial Consumer Chemical Products Under the Consumer Chemical Products and Biocide Safety Management Act (K-BPR). Mass Spectrometry Letters, 10(4), 112-116, https://doi.org/10.5478/MSL.2019.10.4.112

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Abstract

In this study, a chloroform consumer chemical product (CCP) reference material (RM) is successfully developed, with potential to be used in the proficiency testing of hazardous compounds in CCPs for analysis and testing agencies. Validation experiments are rigorously conducted to evaluate whether the RM meets the requirements set by the ISO 13528 and ISO Guide 35, using a reliable GC/MS method for the analysis of chloroform. The obtained calibration plot linearity, limit of detection (LOD), and limit of quantitation (LOQ) are excellent. The developed RM meets the homogeneity and stability requirements; the between-unit (s bb ) and within-unit (s wb ) standard deviations are less than 2.5%, and the stability is found to be guaranteed for 50 days.

keywords: chloroform, reference material, GC/MS, consumer chemical products, biocides

Reference

Alavanja, M. C. R. (2010). . Rev. Environ. Health, 24, 303-.

Trantallidi, M. (2015). . Sci. Total Environ, 536, 903-.

Kwon, K.-D. (2018). . Environ. Sci. Pollut. Res, 15, 521-.

Lee, J. H. (2012). . Environ. Sci. Technol, 46, 2498-.

Hwang, H. J.; Nam, J. J.; Yang, S. I.; Kwon, J.-H.; Oh, H. B.. (2013). MALDI-TOF Analysis of Polyhexamethylene Guanidine (PHMG) Oligomers Used as a Commercial Antibacterial Humidifier Disinfectant. Bulletin of the Korean Chemical Society, 34(6), 1708-1714. http://dx.doi.org/10.5012/bkcs.2013.34.6.1708.

Yoon, D. H. (2015). . Rapid Commun. Mass Spectrom, 29, 213-.

Park, D.-U. (2015). . Indoor Air, 25, 631-.

Kim, H.-R. (2016). . J. Toxic. Sci, 41, 711-.

Bae, J. U. (2019). . Int. J. Mass Spectrom, 435, 298-.

Kupiec, K.. (2009). . Crit. Rev. Anal. Chem, 39, 311-.

Kie basa, A.. (2016). . J. Crit. Rev. Anal. Chem, 46, 224-.

International Organization for Standardization. Statistical methods for use in proficiency testing by interlaboratory comparisons, ISO 13528, 1st ed.

International Organization for Standardization. (2017). Reference materials–Guidance for characterization and assessment of homogeneity and stability, ISO Guide 35, 4th ed:International Organization for Standardization.

Fiss, E. M.. (2007). . J. Environ. Sci. Technol, 41, 2387-.

International Agency for Research on Cancer. IARC Monographs on the Evaluation of Carcinogenic Risks to Humans, Vol. 98.

National Institute of Environmental Research. Regulation on the Criteria and Methods of Testing and Inspection of the Safety Confirmation Targeted Consumer Chemical Products, Vol. 2018-71.

Kim, J.-H.; Choi, S.-G.; Oh, Y.-G.; Hong, S.-M.; Kim, S.-B.; Woo, I.-D.; Kim, J.-Y.; Seo, J.-S.. (2016). Development of Analytical Reference Material for Proficiency Test of Pesticide Multi-residue Analysis in Tomato. Korean Journal of Environmental Agriculture, 35(3), 223-233. http://dx.doi.org/10.5338/KJEA.2016.35.3.24.