- P-ISSN 1225-0163
- E-ISSN 2288-8985
- 권한신청
- P-ISSN1225-0163
- E-ISSN2288-8985
- SCOPUS, ESCI, KCI
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Self assembly directed synthesis of tubular conduction polymer inside th channels of MCM-41
분석과학 / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2006, v.19 no.3, pp.211-217
(경북대학교)
(경북대학교)
(경북대학교)
(경북대학교)
(경북대학교)
(한남대학교)
(경북대학교)
(경북대학교)
(경북대학교)
(경북대학교)
(한남대학교)
Ali,
M.
S.
,
Kwang-Pill,
L.
,
Anantha,
I.
G.
,
K,
R.
R.
,
Sang-Ho,
K.
,
&
최성호.
(2006). . 분석과학, 19(3), 211-217.
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Abstract
Diphenyl amine (DPA) was polymerized inside the channels of the mesoporous silica (MCM-41). MCM-41 (C) and MCM-41 (D) were prepared with cetyltrimethyl ammonium bromide (CTAB) and dodecyltrimethyl ammonium bromide (DTAB), respectively and used as hosts. Initially, the self assembly of DPA inside the pores of MCM-41 was made in β-naphthalene sulfonic acid (NSA) medium and subsequently poly (diphenylamine), PDPA was formed by oxidative polymerization. N2 adsorption-desorption measurements of PDPA loaded MCM-41 (C) and MCM-41 (D) show variations in pore volume and surface area between them. A tubular form of poly (diphenylamine), PDPA was envisaged to form in the pores of MCM-41 and supported by high resolution transmission microscopy. The presence of PDPA inside the channel of MCM-41 was further confirmed by FTIR spectroscopy, thermogravimetric analysis (TGA), X-ray diffraction.
- keywords
- Mesoporous silica (MCM-41), poly (diphenylamine), self-assembly
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