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- E-ISSN 2288-8985
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- P-ISSN1225-0163
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Adsorptive Stripping Voltammetrical Determination of Zirconium
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
1993, v.6 no.5, pp.425-433
Choi,
W. H., Lee,
J. S., Kim,
D. H., &
Kim,
J.
C.
(1993). Adsorptive Stripping Voltammetrical Determination of Zirconium. Analytical Science and Technology, 6(5), 425-433.
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Abstract
Adsorptive stripping voltammetric determination method of trace zirconium using oxine as a ligand was studied. Optimal conditions found to be <TEX>$2.5{\times}10^{-3}M$</TEX> borax buffer solution(pH 8.5) containing oxine concentration of <TEX>$4{\times}10^{-8}M$</TEX>. Accumulation potential was -0.2V, accumulation time was 400sec and scan rate was 4mV/sec. Calibration plots for zirconium are linear over the range of <TEX>$1{\sim}100{\mu}g/L$</TEX> in optimal condition.
- keywords
- Zirconium, Oxine, Adsorptive Stripping Voltammetry
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