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  • P-ISSN 1225-0163
  • E-ISSN 2288-8985

Determination of bisphenol-A using GC/MS in Can Materials

Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2001, v.14 no.6, pp.499-503
Kim, Ki-Cheol
Kim, Yang-Hee
Choi, Ok-Kyung
Ko, Hoan-Uck
Yim, Jun-Rae
Choi, Kyo-Hong
Cho, Hyun-Woo
Kim, Hye-Young
Kim, Myungsoo
Myung, Seung-Woon
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Abstract

A new simple, rapid and sensitive gas chromatographic technique for the determination of bisphenol-A in can materials, which is the major material of epoxy resin and polycarbonate polymer, is proposed. This method is characterised by derivatization of the bisphenol-A with a acylating reagent forming the acetate derivative to optimize the chromatographic property. The detection of bisphenol-A is performed based on GC/MS (gas chromatography/mass spectrometry). Several beverages were analyzed by the proposed method for the determination of bisphenol-A Bisphenol-A was assayed the range of <TEX>$0.11{\sim}11.40{\mu}g/can$</TEX> from the can materials.

keywords
endocrine disruptors, bisphenol-A, GC/MS, can materials


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