- P-ISSN 1225-0163
- E-ISSN 2288-8985
- P-ISSN1225-0163
- E-ISSN2288-8985
- SCOPUS, ESCI, KCI
Article Detail
Home > Article Detail
Analysis of mercury and methylmercury in river sediment samples
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2009, v.22 no.1, pp.44-50
&
(2009). Analysis of mercury and methylmercury in river sediment samples. Analytical Science and Technology, 22(1), 44-50.
- Downloaded
- Viewed
Abstract
In this study, the use of purge & trap GC-MS technique for determination of methylmercury in sediment samples was described. The method detection limit of the method was determined as 0.06 ng/g and the recovery of the method was 102±11.4%, with precisions better than 11.2%. The method was validated by analysis of CRMs such as ERM CC580 (estuarine sediment) and IAEA 405 (sediment). Additionally, the performance of the method was tested on river sediment samples and the analytical results were compared with those of the GC-CVAFS, which has been widely used for methylmercury analysis.
- keywords
- methylmercury, mercury, distillation technique, purge & trap gc-ms, sediment
Reference
1
1. USEPA, ‘Mercury study report to Congress. Vol. V. Health effects of mercury and mercury compounds’, December, 1997.
2
2. UNEP Chemical, ‘Global Mercury Assessment. December. UNEP Chemicals’, part of UNEP's Technology, Industry and Economics Division, 2002.
3
3. R. P. Mason, N. N. Lawson, A. L. Lawrence, J. J. Leaner, J. G. Lee and G.-R. Sheu, Mar. Chem., 65, 77-96(1999).
4
4. P. R. Mason and A. L. Lawrence, Environmental Toxicology and Chemistry, 18(11), 2438-2447(1999).
5
5. C. J. Henny, E. F. Hill, D. J. Hoffman, M. G. Spalding and R. A. Grove, Ecotoxicology, 11, 213-231(2002).
6
6. D. Mergler, H. A. Anderson, L. H. M. Chan, K. R. Mahaffey, M. Murray and M. Sakamoto, Ambio, 36, 3- 11(2007).
7
7. D. W. Boening, Chemosphere, 40, 1335-1351(2000).
8
8. USEPA, Water Quality Criterion for the Protection of Human Health : Methylmercury, EPA-823-R-01-001 (2001).
9
9. 환경부, ‘국민 혈중의 중금속 농도 조사·연구’, 2005.
10
10. 국립환경과학원, ‘환경매체별 유기수은 시험방법 확립 및 분포현상 연구(II)’, 2007.
11
11. USEPA method 1630, ‘Methylmercury in water by distillation, aqueous ethylation, purge and trap, and CVAFS’, 2001.
12
12. J. S. Lee, Y. J. Ryu, J. S. Park, S. H. Jeon, S. C. Kim and Y. H. Kim, Bull. Kor. Chem. Soc., 58, 2293-2298(2007).
13
13. Ph. Quevauviller, G. U. Fortunati, M. Filippelli and H. Muntau, 'The certification of the contents (mass fractions) of total mercury and methylmercury in estuarine sediment CRM 580', EUR 17658 EN, 1997.
14
14. C. R. Hammerschmidt and W. F. Fitzgerald, Anal. Chem., 73, 5930-5936(2001).
15
15. 어수미, ‘서울시 인근의 한강 본류 및 지류에 대한 하상 저질의 중금속 오염평가’, 서울대학교 박사학위 논문, 1994.
16
16. J. M. Benoit, C. C. Gilmour, A. Heyes, P. R. Mason and C. Miller, ‘Biochemistry of environmental important trace elements. American Chemical Society’, Washington, DC, 262-297(2003).
17
17. A. Heyes, R. P. Mason, E-. H. Kim and E. Sunderland, Mar. Chem., 102, 134-147(2006).
18
18. J. M. Benoit, C. C. Gilmour, R. P. Mason, G. S. Riedel, G. F. Reidel and K. A. Sullivan, Biogeochemistry, 40, 249-265(1998).
Other articles from this issue
- Process analytical technology (PAT): field applications and current status in pharmaceutical industries
- Analysis of mercury and methylmercury in river sediment samples
- Age comparisons of coastal sand dune stratum in Chollipo, Korea by altering preheat and cut-heat, and grain size distributions by OSL dating
- Development of a building materials database; Volatile organic compounds, formaldehyde emission rates and chemical compositions
- The analysis of the urushiol congeners from the extracts of lacquer trees
- Study on the size-based separation of nano to micron particles in natural water and soil using flow and sedimentation Field-flow fractionation
- Preparation and evalution of limestone reference material for a proficiency test
- Adsorption of uranium(Ⅵ), calcium(Ⅱ), and samarium(Ⅲ) ions on synthetic resin adsorbent with styrene hazardous materials
- Bioequivalence of pioglitazone tablet to Actos® tablet(Pioglitazone 30 mg)
- Analysis of polycyclic aromatic hydrocarbons in cooked fish and shellfish
- more
Recommanded Articles
This website recommended the use the Chrome browser for journal website.