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- E-ISSN 2288-8985
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- E-ISSN2288-8985
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Determination of volatile compounds by headspace-solid phase microextraction – gas chromatography / mass spectrometry: Quality evaluation of Fuji apple
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2017, v.30 no.2, pp.68-74
https://doi.org/10.5806/AST.2017.30.2.68
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(2017). Determination of volatile compounds by headspace-solid phase microextraction – gas chromatography / mass spectrometry: Quality evaluation of Fuji apple. Analytical Science and Technology, 30(2), 68-74, https://doi.org/10.5806/AST.2017.30.2.68
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Abstract
The volatile components in ‘Fuji’ apple were effectively determined by a headspace solid-phase microextraction (HS-SPME) combined with gas chromatography-mass spectrometry (GC-MS). A total of 48 volatile components were identified and tentatively characterized based on National Institute of Standards and Technology (NIST) MS spectra library and the Kovats GC retention index I (RI). The harvested Fuji apples were divided into two groups: 1-methylcyclopropene (1-MCP) treated and non-treated (control) samples for finding important indicators between two groups. The major volatile components of both apples were 2-methylbutyl acetate, hexyl acetate, butyl 2-methylbutanoate, hexyl butanoate, hexyl 2-methylbutanoate, hexyl hexanoate and farnesene. No significant differences of these major compounds between 1-MCP treated and non-treated apples were observed during 1 month storage. Interestingly, the amount of off-flavors, including 1-butanol and butyl butanoate, in 1-MCP treated apples decreased over 5 months, and then increased after 7 months. However, non-treated apples did not show significant changes for off-flavors during 7 month storage (p<0.05). The non-treated apples also contained the higher levels of two off-flavors than 1-MCP treated apples. These two compounds,
- keywords
- Fuji apples, volatile compounds, off-flavors, HS-SPME/GC-MS
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