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- E-ISSN 2288-8985
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Establishment and validation of an analytical method for quality control of health functional foods derived from Agastache rugosa
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2019, v.32 no.3, pp.96-104
https://doi.org/10.5806/AST.2019.32.3.96
(School of Pharmacy, Sungkyunkwan University)
(School of Pharmacy, Sungkyunkwan University)
(School of Pharmacy, Sungkyunkwan University)
(COSMAX NS Inc.,)
(COSMAX NBT Inc)
(School of Pharmacy, Sungkyunkwan University)
(School of Pharmacy, Sungkyunkwan University)
(School of Pharmacy, Sungkyunkwan University)
(COSMAX NS Inc.,)
(COSMAX NBT Inc)
(School of Pharmacy, Sungkyunkwan University)
Keunbae,
P.
, Dasom,
J.
, Yan,
J.
, Jin,
H.
K.
, Jeong,
H.
G.
, &
Jeongmi,
L.
(2019). Establishment and validation of an analytical method for quality control of health functional foods derived from Agastache rugosa. Analytical Science and Technology, 32(3), 96-104, https://doi.org/10.5806/AST.2019.32.3.96
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Abstract
Agastache rugosa, known as Korean mint, is a medicinal plant with many beneficial health effects. In this study, a simple and reliable HPLC-UV method was proposed for the quantification of rosmarinic acid (RA) in the aqueous extracts of A. rugosa. RA was selected as a quantification marker due to its easiness in procurement and analysis. The developed method involved chromatographic separation on a C18 column (250 × 4.6 mm, 5 μm) at room temperature. The mobile phase consisted of water and acetonitrile both containing 2 % acetic acid and was run at a flow rate of 1 mL min−1. The method was validated for specificity, linearity, precision, and accuracy. It was specific to RA and linear in the range of 50–300 μg mL−1 (r2 = 0.9994). Intraday, inter-day, and inter-analyst precisions were ≤ 0.91 % RSD, ≤ 1.40 % RSD, and 1.94 % RSD, respectively. Accuracy was 93.3–95.9 % (≤ 1.21 % RSD). The method could be applied to three batches of bulk samples and three batches of lab scale samples, which were found to be 0.64 (± 0.04) mg g−1 and 0.48 (± 0.02) mg g−1 for the dried raw materials of A. rugosa. The results show that the proposed method can be used as a readily applicable method for QC of health functional foods containing the aqueous extracts of A. rugosa.
- keywords
- Agastache rugosa, rosmarinic acid, health functional food, quality control
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