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  • P-ISSN1225-0163
  • E-ISSN2288-8985
  • SCOPUS, ESCI, KCI

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  • P-ISSN 1225-0163
  • E-ISSN 2288-8985

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    REACH 물질 등록 시 분류에 영향을 주는 미량 유해 무기물질의 스크리닝·정량·해석을 위한 체계도 연구

    Study on scheme for screening, quantification and interpretation of trace amounts of hazardous inorganic substances influencing hazard classification of a substance in REACH registration

    분석과학 / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
    2019, v.32 no.6, pp.233-242
    https://doi.org/10.5806/AST.2019.32.6.233
    권현아 (한국생산기술연구원 환경규제기술센터)
    박광서 (한국생산기술연구원 환경규제기술센터)
    손승환 (한국생산기술연구원 환경규제기술센터)
    최은경 (한국생산기술연구원 환경규제기술센터)
    김상헌 (경성대학교 공과대학 제약공학과, 화학안전연구센터)
    권현아, 박광서, 손승환, 최은경, & 김상헌. (2019). REACH 물질 등록 시 분류에 영향을 주는 미량 유해 무기물질의 스크리닝·정량·해석을 위한 체계도 연구. 분석과학, 32(6), 233-242, https://doi.org/10.5806/AST.2019.32.6.233
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    Abstract

    Substance identification is the first step of the REACH registration. It is essential in terms of Classification, Labelling and Packaging (CLP) regulation and because even trace amounts of impurities or additives can affect the classification. In this study, a scheme for the screening, quantification, and interpretation of trace amounts of hazardous inorganic substances is proposed to detect the presence of more than 0.1% hazardous inorganic substances that have been affecting the hazard classification. An exemplary list of hazardous inorganic substances was created from the substances of very high concern (SVHCs) in REACH. Among 201 SVHCs, there were 67 inorganic SVHCs containing at least one or ~2-3 heavy metals, such as As, Cd, Co, Cr, Pb, Sb, and Sn, in their molecular formula. The inorganic SVHCs are listed in excel format with a search function for these heavy metals so that the hazardous inorganic substances, including each heavy metal and the calculated ratio of its atomic weight to molecular weight of the hazardous inorganic substance containing it, can be searched. The case study was conducted to confirm the validity of the established scheme with zinc oxide (ZnO). In a substance that is made of ZnO, Pb was screened by XRF analysis and measured to be 0.04% (w/w) by ICP-OES analysis. After referring to the list, the presence of Pb was interpreted just as an impurity, but not as an impurity relevant for the classification. Future studies are needed to expand on this exemplary list of hazardous inorganic substances using proper regulatory data sources.

    keywords
    REACH, substance identification, classification, hazardous inorganic substance, heavy metals


    참고문헌

    1

    1. REACH 2018 registration statics, European Chemicals Agency, September 2018.

    2

    2. EU REGULATION (EC) No 1907/2006, Registration, Evaluation, Authorisation and Restriction of Chemicals (REACH), 2006 (Document 02006R1907-20190107).

    3

    3. Guidance on registration, European Chemicals Agency, Version 3.0, November 2016.

    4

    4. Guidance on data-sharing, European Chemicals Agency, Version 3.1, January 2017.

    5

    5. Guidance for identification and naming of substances under REACH and CLP, European Chemicals Agency, Version 2.1, May 2017.

    6

    6. Introductory guidance on the CLP regulation, European Chemicals Agency, Version 3.0, January 2019.

    7

    7. Guidance on the preparation of dossiers for harmonized classfication and labelling, Version 2.0, August 2014.

    8

    8. Guidance on the Application of the CLP Criteria. European Chemicals Agency, Version 5.0. July 2017.

    9

    9. How to gather information to register a multi-constituent or a UVCB substance-toxicological information, European Chemicals Agency, December 2017.

    10

    10. EU REGULATION (EC) No 1272/2008 on classification, labelling, and packaging of substances and mixtures, 2008.

    11

    11. Substances of very high concern identification https://echa.europa.eu/substances-of-very-high-concern-identification, Assessed 25 July 2019.

    12

    12. Authorisation, https://echa.europa.eu/substances-of-veryhigh-concern-identification-explained, Assessed 25 July 2019.

    13

    13. Candidate list of substances of very high concern for authorisation, http://echa.europa.eu/candidate-list-table, Assessed 25 July 2019.

    14

    14. KS M 8107:2005, Zinc oxide, Korean Standards Association, 2018 (Last updated).

    15

    15. IEC 62321-5, Cadmium, lead and chromium in polymers and electronics and cadmium and lead in metals by AAS, AFS, ICP-OES and ICP-MS, Edition 1.0, 2013.

    16

    16. Report to the NIER, 환경측정분석 정도관리를 위한표준물질 제조 및 보급-토양분석용 중금속 표준물질, Korea Research Institute of Standards and Science, 2008.

    17

    17. Zinc REACH Consortium: Zinc oxide (EC215-222-5), https://www.reach-zinc.eu/sief-page/welcome-to-the-siefsubstances-page/zinc-oxide-ec-2152225, Assessed 25July 2019.

    18

    18. Classification: Agents classified by the IARC monographs, volumes 1–124, http://monographs.iarc.fr/ENG/Classification/index.php, Assessed 25 July 2019.

    19

    19. Search the SIN list, https://sinlist.chemsec.org/search/searchall, Assessed 25 July 2019.

    20

    20. Table of harmonised entries in Annex VI to CLP, https://echa.europa.eu/information-on-chemicals/annexvi-to-clp, Assessed 25 July 2019.

    21

    21. CMR substances fron Annex VI of the CLP Regulation registered under REACH and notified under CLP, European Chemicals Agency, 2012.

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