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Development of Analytical Techniques for Human Serum and Urine by Using Glow Discharge
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
1998, v.11 no.3, pp.167-173
Lee,
S. C., Choi,
K., Son,
E., &
Sim,
Y.
(1998). Development of Analytical Techniques for Human Serum and Urine by Using Glow Discharge. Analytical Science and Technology, 11(3), 167-173.
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Abstract
An electrothermal vaporization-hollow cathode glow discharge-atomic emission spectrometer(ETV-HCGD-AES) has been developed for detecting heavy metals in human serum and urine samples. Fisrt of all, we designed a glow discharge cell for atomic emission spectrometry and its analytical performance was studied with the standard reference materials(SRMs) purchased from the NIST. Practically, the ETV-HCGD-AES demonstrated better instrumental sensitivity and selectivity for detecting Hg and Pb in the SRMs, serum and urine, than ICP-OES since the ETV-HCGD-AES was not required the complicate sample digestion procedure, which improved sample transportation efficiency.
- keywords
- Hollow cathode glow discharge, Atomic emission spectrometry, Urine and serume analysis
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