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Determination of Volatile Organic Compounds in Waste using HS/GC/MS Analysis
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2000, v.13 no.1, pp.72-80
Kim,
K., Shin,
S., &
Ju,
D.
(2000). Determination of Volatile Organic Compounds in Waste using HS/GC/MS Analysis. Analytical Science and Technology, 13(1), 72-80.
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Abstract
The HS/GC/MS method was performed to analyze the volatile organic compounds in waste sludge samples. This study was performed to establish the fundamental data by studying the effects of salt, equilibrium temperature and time in the volatile organic compounds analysis. The presence of salts have been found to increase the sensitivity. The peak area is increased from 1.07 to 2.61 times by adding the salts to the water sample, compared with a salt tree sample. The recoveries of target compounds have found between 90% and 127% at sample temperature of <TEX>$85^{\circ}C$</TEX> for 30 min. This HS/GC/MS method can be applied to analyze the volatile organic compounds and organohalo compounds in the environmental matrix.
- keywords
- headspace analysis, volatile organic compounds
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