- P-ISSN 1225-0163
- E-ISSN 2288-8985
- P-ISSN1225-0163
- E-ISSN2288-8985
- SCOPUS, ESCI, KCI
Article Detail
Home > Article Detail
Quantitative analysis of 3-MCPD in water using LC-MS
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2007, v.20 no.3, pp.198-203
&
(2007). Quantitative analysis of 3-MCPD in water using LC-MS. Analytical Science and Technology, 20(3), 198-203.
- Downloaded
- Viewed
Abstract
The analysis method of 3-Monochloropropane-1,2-diol (3-MCPD) compound in water was developed using liquid chromatography with mass spectrometric detection. Aqueous solution was controlled in strong basic condition with sodium hydroxide, and then <TEX>$25{\mu}L$</TEX> of benzoyl chloride was added to the solution for the derivatization of 3-MCPD. The derivative was extracted using pentane and analyzed by the selected ion monitoring (SIM) method of LC-MS. The results of analyses showed that the calibration curves was in the range of 1.0 to <TEX>$100{\mu}g/mL$</TEX> with a good linearity (correlation coefficient of <TEX>$r^2
- keywords
- 3-Monochloropropane-1, 2-diol, 3-MCPD, LC-MS. benzoyl chloride
Reference
1
C.G. Hamlet, (1998) Food Addit,
Other articles from this issue
- Proficiency testing of cadmium and lead in polypropylene resin
- Adsorption of phenol on metal treated by granular activated carbon
- Quantitative analysis of 3-MCPD in water using LC-MS
- Study on the confirmation of drinking at the bloods & urines used 5-hydroxyindole-3-acetic acid and 5-hydroxytryptophol
- Determination of Copper(II) ion with a nafion-ethylenediamine modified glassy carbon electrode
- Natural isotopes and trace element analyses in glass samples
- Contents of lead, mercury, and cadmium in seaweeds collected in coastal area of Korea
- Determination of the presence of benzene in vitamin drinks using headspace - solid phase microextraction and gas chromatography - mass spectrometry
- Separation and analysis of Cr(III) and Cr(VI) using 8-hydroxyquinoline complexation of Cr(III)
- Determination of osmium using sulfurous acid as reductant by ICP-AES
- Simultaneous determination of low molecular weight amines and quaternary ammonium ions by IC/ESI-MS
- more
Recommanded Articles
This website recommended the use the Chrome browser for journal website.