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Simultaneous and quantitative determination of anion biocides in soil by liquid chromatography-tandem mass spectrometry
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2015, v.28 no.5, pp.317-322
https://doi.org/10.5806/AST.2015.28.5.317
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(2015). Simultaneous and quantitative determination of anion biocides in soil by liquid chromatography-tandem mass spectrometry. Analytical Science and Technology, 28(5), 317-322, https://doi.org/10.5806/AST.2015.28.5.317
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Abstract
토양 중 음이온 바이오사이드인 chlorite, chlorate, cyanuric acid와 sodium dodecylbenzenesulfonate (Na-DBS)의 liquid chromatography-tandem mass spectrometry (LC-MS/MS) 동시 분석방법을 개발하였다. Chlorite와 chlorate는 물로 추출하였으며, cyanuric acid와 Na-DBS는 0.25 mM ammonium formate를 함유한 20 mM formic acid와 acetonitrile (1:1) 이동상을 이용하여 추출하였다. 추출물은 필터 후 직접 LCMS/ MS로 주입하였다. 분석물질이 검출되지 않는 토양에 각 성분들을 첨가한 후 정도관리를 실시한 결과 검출한계는 chlorite 0.04 mg/kg, chlorate 0.04 mg/kg, cyanuric acid 0.27 mg/kg 그리고 Na-DBS의 경우는 0.05 mg/kg 이었다. 이 방법을 사용하여 우리나라 AI로 소독제를 많이 사용한 장소 40개 지역과 사용하지 않은 지역 10개 대조 지역의 토양을 분석한 결과 대조지역을 포함한 모든 조사지역에서 네 가지음이온 모두 검출되지 않았다.
- keywords
- chlorite, chlorate, cyanuric acid, Na-DBS, soil, LC-MS/MS
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