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Simultaneous determination of bisphenol A, chlorophenols and alkylphenols by solid-phase extraction and HPLC
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2017, v.30 no.1, pp.20-25
https://doi.org/10.5806/AST.2017.30.1.20
(Gangwondo Institute of Health and Environment)
(Gangwondo Institute of Health and Environment)
(Gangwondo Institute of Health and Environment)
&
(2017). Simultaneous determination of bisphenol A, chlorophenols and alkylphenols by solid-phase extraction and HPLC. Analytical Science and Technology, 30(1), 20-25, https://doi.org/10.5806/AST.2017.30.1.20
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Abstract
An analytical method for determining potential endocrine disruptors (bisphenol A, 2-chlorophenol, 2,4-dichlorophenol, 2,4,6-trichlorophenol, pentachlorophenol, p-t-butylphenol, p-pentylphenol, p-hexylphenol, pt- octylphenol, p-heptylphenol, nonylphenol) by solid-phase extraction (SPE) and High Perfomance Liquid Chromatography(HPLC) equipped with fluorescence and variable wavelength detector has been developed. The SPE process for sample concentration was performed on a commercially available Oasis HLB cartridge packed with polymeric sorbents. The effect of elution solvent and elution volume on the recoveries of the analytes were investigated with HPLC. Average recovery of >85% was achieved with 60mg sorbents using 5mL of methanol as elution solvent. Phenolic compounds in canned drinks, beverages and water samples were surveyed by this proposed method.
- keywords
- bisphenol A, alkylphenols, chlorophenols, high performance liquid chromathgraphy (HPLC), solid phase extraction (SPE)
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