- P-ISSN 1225-0163
- E-ISSN 2288-8985
- Log In/Sign Up
- P-ISSN1225-0163
- E-ISSN2288-8985
- SCOPUS, ESCI, KCI
Article Detail
Home > Article Detail
Synthesis, crystal structure, and analytical characterizations of amphiphilic palladium(II) compound containing bis(benzylthio)methylenepropanedioate
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2023, v.36 no.4, pp.198-203
https://doi.org/10.5806/AST.2023.36.4.198
(Department of Chemistry Education and Institute of Fusion Science, Jeonbuk National University)
Tae,
H.
N.
(2023). Synthesis, crystal structure, and analytical characterizations of amphiphilic palladium(II) compound containing bis(benzylthio)methylenepropanedioate. Analytical Science and Technology, 36(4), 198-203, https://doi.org/10.5806/AST.2023.36.4.198
- Downloaded
- Viewed
Abstract
The reaction of cis-protected (Me4en)Pd(II) species with potentially multidentate bis(benzylthio)methylenepropanedioate (L) was carried out to obtain a monometallic compound, [(Me4en)Pd(L)], in O,O’-coordination mode. The bis(benzylthio)methylene group was bent strikingly from the palladium square plane at the dihedral angle of 70.40°. The physicochemical properties of the present palladium(II) compound were fully characterized by means of infrared and nuclear magnetic resonance spectroscopy, thermogravimetric analysis, and single-crystal X-ray diffraction measurement.
- keywords
- coordination mode, crystal engineering, X-ray diffraction, NMR spectroscopy
Other articles from this issue
- Liquid chromatographic enantioseparation of several amino acids as nitrobenzoxadiazole derivatives on polysaccharide trisphenylcarbamate derived chiral stationary phases
- Optimization and validation of HPLC/DAD method for the determination of adenosine and cordycepin in cordyceps products
- Detection of Al3+ by fluorescent turn-on nitrogen/sulphur-binary doped carbon dots
- Correlation of ketone bodies in blood and spleen
- Qualitative and quantitative assessment of process related impurities in Brigatinib raw material and formulations using HPLC
- Radioactivity concentrations of natural radionuclides in fine dust of Jeju, Korea
- Synthesis, crystal structure, and analytical characterizations of amphiphilic palladium(II) compound containing bis(benzylthio)methylenepropanedioate
- Erratum : Problem-solving approach for salbutamol analysis by HPLC during pharmaceutical assay
- more
Recommanded Articles
This website recommended the use the Chrome browser for journal website.