- P-ISSN 1225-0163
- E-ISSN 2288-8985
- Log In/Sign Up
- P-ISSN1225-0163
- E-ISSN2288-8985
- SCOPUS, ESCI, KCI
Article Detail
Home > Article Detail
A Study on the Racemization of Amino acids and its Separation with GC, GC/MS and HPLC
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
1994, v.7 no.1, pp.41-52
Rhee,
J., Hong,
J., Eo,
Y., &
Kim,
T.
(1994). A Study on the Racemization of Amino acids and its Separation with GC, GC/MS and HPLC. Analytical Science and Technology, 7(1), 41-52.
- Downloaded
- Viewed
Abstract
The importance of separation comes from demands on study for exact effect of synthetic drugs and the reactivity of enantiomer in biological system. Racemization rate was measured under the influence of heat, acid, UV-light, enzyme(trypsin) and 6N-HCl at <TEX>$105^{\circ}C$</TEX> on alanine, threonine, isoleucine, lecuine, aspartic acid, methionine, glutamic acid, tyrosine. The method for the identification of overlapped amino acids with GC was developed from the close study of fragmentation pattern with mass spectrometry. With cyclodextrin bonded phase by HPLC, the separation of dansyl amino acid was tested for compartison.
- keywords
- Amino acids, enantiomer, Mass spectrometry, HPLC, cyclodextrin
- Downloaded
- Viewed
- 0KCI Citations
- 0WOS Citations
Other articles from this issue
- The analysis of impurities in rare earth oxide for fluorescent substance by ICP-MS
- A Study On Chemical Composition of Saururaceae Growing in Korea(5) On Flavonoid Constituents of Saururus Chinensis
- A Study on the Charateristics of ORMOSIL as a Dye Host by Measurement of UV/VIS Spectrophotometer
- A Study on the Development of Analytical Methods and Behaviors of Environmental Pollutants(II) : Optimization for Separation of Alkylphenols by Reversed-Phase Liquid Chromatography
- A Study on the Development of Analytical Methods and Behaviors of Environmental Pollutants(III) : On-Line System for Preconcentration and Separation of Trace Phenols by HPLC
- A Study on the Racemization of Amino acids and its Separation with GC, GC/MS and HPLC
- A Study on the Separation of Racemic Amino acids in Food or Biological Sample with GLC
- Simultaneous Analysis of Triazines and Phenoxyalkanoic Acids by GC/MS
- Studies on the effect of the intermolecular hydrogen bonding on the vibrational frequencies of the acetonitrile under matrix isolation conditions at liquid-<TEX>$N_2$</TEX> temperature
- <TEX>$A^{13}$</TEX> CNMR Determination of Monomer Composition in EP Copolymers, EPB and EPDM Terpolymers
- Separation and Elution Behaviors of Some Metal-2-hydroxyarylazopyrazolone Chelates by Reversed Phase High Performance Liquid Chromatography (I)
- Surface Analysis of Cold Rolled Steel Sheets by X-ray Photoelectron Spectroscopy
- A Study on the Analysis of Volatile Flavour of Kimchee
- more
Recommanded Articles
This website recommended the use the Chrome browser for journal website.