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Effect of Fluoride Ion in the Analysis of Tin by HG-ICP-AES
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2001, v.14 no.5, pp.416-421
Lim,
H., Cho,
S., &
Lee,
S.
(2001). Effect of Fluoride Ion in the Analysis of Tin by HG-ICP-AES. Analytical Science and Technology, 14(5), 416-421.
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Abstract
The optimization of the reductant and acid concentration for stannane(<TEX>$SnH_4$</TEX>) generation was investigated by using a continuous flow hydride generator combined with an inductively coupled plasma-atomic emission spectrometer. Several different prereductants were studied to remove the interfering effect of fluoride ion on the hydride generating of tin. The optimum acid concentration was 0.5-1.0 M for the 1-2% <TEX>$NaBH_4$</TEX> and 1.0 M NaOH and the interfering effect of fluoride ion was minimized using boric acid and L-cysteine mixed solution as a prereductant. The reconveries of tin at 20 ng/mL level in the solution containing fluoride ion were 100~108 %.
- keywords
- tin, HG-ICP-AES, fluoride ion, prereductant effect
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