- P-ISSN 1225-0163
- E-ISSN 2288-8985
- Log In/Sign Up
- P-ISSN1225-0163
- E-ISSN2288-8985
- SCOPUS, ESCI, KCI
Article Detail
Home > Article Detail
Determination of Plutonium in HANARO Irradiated Fuel by IDMS
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2003, v.16 no.3, pp.191-197
&
(2003). Determination of Plutonium in HANARO Irradiated Fuel by IDMS. Analytical Science and Technology, 16(3), 191-197.
- Downloaded
- Viewed
Abstract
Two methods, IDMS (Isotope Dilution Mass Spectrometry) and controlled potential coulometry are compared by the determination of Pu for the NBL, CRM No.122, <TEX>$PuO_2$</TEX>. The recovery of Pu was found to be <TEX>$1.002176{\pm}0.000452$</TEX> within the relative standard deviation of 0.045% (95% conf. level) although a small size of sample (<TEX>$0.9{\mu}g$</TEX>-Pu) was used in IDMS. The recovery using controlled potential coulometry were obtained in the range of 0.9923~0.9960. The analytical results of IDMS and controlled potential coulometry were good agreement within 0.6~1%. Base on these experiment results, The plutonium in HANARO irradiated fuel rod that separated portion of top, middle, and bottom were determined. The measured values of Pu are 1.155 mg, 2.483 mg and 1.920 mg in one gram of sample(fuel+clad), respectively.
- keywords
- plutonium, IDMS, irradiated fuel, coulometry
Other articles from this issue
- Separation and purification of substance having matrix metalloproteinase-9 inhibition effect in Ulmus davidiana Plancn. Var. japonica Nkai.
- A Study on the Treatment of Uncertainty in Linear Regression Method for Chemical Analysis
- Determination of Plutonium in HANARO Irradiated Fuel by IDMS
- Electrochemical behavior and Application of Osmium-Cupferron Complex
- Study on Dc Polarograms of Some Rare Earth Elements
- Memory Effect of Silver and Aqua Regia by their Permeation into Microwave Digestion Vessels
- Study on the Treatment of Hydrogen Chlorde Gas used in Semiconductor Process by using Gas Adsorptioj Agents such as Zeolite Resins, AnO, and AgMnO3
- Development of AAS and Determination of metals in airborne particiles.
- Study on Distribution of Elemental Concentration with a Different Depth of River Sediment using Neutron Activation Analysis
- A Study on the Distribution of Atmospheric Concentrations of Sulfur Compounds by GC/FPD
- A Study on Formation Pattern of DBPs by Disinfection of Drinkig Raw Water
- more
Recommanded Articles
This website recommended the use the Chrome browser for journal website.