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- E-ISSN 2288-8985
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- P-ISSN1225-0163
- E-ISSN2288-8985
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Memory Effect of Silver and Aqua Regia by their Permeation into Microwave Digestion Vessels
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2003, v.16 no.3, pp.212-217
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(2003). Memory Effect of Silver and Aqua Regia by their Permeation into Microwave Digestion Vessels. Analytical Science and Technology, 16(3), 212-217.
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Abstract
The memory effect of silver and aqua regia in the vessel by their permeation was studied during the microwave digestion of samples under the operating conditions of high temperature and pressure. The extent of permeation in vessels with the solution containing silver 5 mg has been shown to be <TEX>$0.97{\mu}g/mL$</TEX> for the digestion of <TEX>$HNO_3$</TEX> solution and <TEX>$0.47{\mu}g/mL$</TEX> for the digestion of oil sample under condition of MDS 180T program (<TEX>$180^{\circ}C$</TEX>, 220 psi).
- keywords
- memory effect, microwave digestion, permeation, aqua regia, silver
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