- P-ISSN 1225-0163
- E-ISSN 2288-8985
- P-ISSN1225-0163
- E-ISSN2288-8985
- SCOPUS, ESCI, KCI
Article Detail
Home > Article Detail
Comparison of Static and Dynamic Solvent Extraction of Polychlorinated Dibenzofurans from Fly Ash
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2004, v.17 no.4, pp.295-301
&
(2004). Comparison of Static and Dynamic Solvent Extraction of Polychlorinated Dibenzofurans from Fly Ash. Analytical Science and Technology, 17(4), 295-301.
- Downloaded
- Viewed
Abstract
In this study, static and dynamic solvent extractions are compared for more efficient extraction of polychlorinated dibenzofurans (PCDFs) from fly ash. Static solvent extraction rather than dynamic extraction showed a higher recovery of PCDFs, which was adsorbed strongly with fly ash. The effects of parameters, such as temperature, toluene-isopropyl alcohol mixture, static and dynamic time flow rate, and solvent volume on the extraction were investigated and the variations in average recoveries of PCDFs were explained. In both extractions, temperature was an effective parameter because the higher temperature gave the higher recoveries. In dynamic solvent extraction, dynamic time was more effective than flow rate and solvent volume for the extraction of PCDFs from fly ash. Multi-layer column chromatography on neutral and acidic silica gel with n-hexane was used for cleaning up the extracts. The quantification of the PCDFs extracted was performed using HPLC-UV.
- keywords
- Static solvent extraction, Dynamic solvent extraction, Fly ash, HPLC-UV
Reference
1
Zuloaga, O, (1999) Talanta,
2
Sulkowski, W, (1999) Chromatogr. A,
3
Luque de Castro, M. D, (1998) Anal. Chim. Acta,
4
Zuluoga, O, (1998) rends in Anal. Chem.,
5
Evans, J, (1998) J. Soil Contamination,
6
McNally, M. E. P, (1995) Anal. Chem.,
7
van Bavel, B, (1996) Anal. Chem,
8
Reighard, T. S, (1996) Anal. Chem.,
9
Cui, Y, (1995) J. Chromatogr. A,
10
Richter, B.E, (1997) Chemosphere,
11
Langenfeld, J.J, (1993) J. Anal. Chem,
12
Langenfeld, J.J, (1995) J. Anal. Chem,
13
Kemmochi, Y, (2001) Chemosphere ,
14
Richter, B.E, (1996) Anal. Chem.,
15
Yang, J. S, (2001) J. Liq. Chrom. & Rel. Technol.,
16
Reindl, S, (1994) Anal. Chem,
17
Hawthorne, S. B, (1993) J. Chromatogr,
18
Langenfeld, J. J, (1992) J. Chromatogr.,
Other articles from this issue
- Determination of oxymatrine in Sophora Radix by High Performance Liquid Chromartography
- Comparison of Static and Dynamic Solvent Extraction of Polychlorinated Dibenzofurans from Fly Ash
- Determination of trace actinide(Am, Pu, Th, U) using alpha spectrometry and neutron activation analysis
- Trace impurities analysis of the electronic polymer resins by neutron activation analysis
- The classification of ballpoint pen inks in Questioned Documents by using VSC and SERRS
- A study on the derivatization technique for tamoxifen metabolites in human urine by gas chromatography/mass spectrometry
- A study of the metabolites for 7-keto-DHEA-acetate in human urine
- Accumulation Levels and Distribution Characteristics of Polychlorinated Biphenyls in Crucians and Leopard Frogs from the Nakdong River Basin
- EPMA Analysis of Inter-reaction Layer in Irradiated U3Si-Al Fuels
- Determination of Heavy Metal in Polyurethane by New Digestion Method and ICP-AES
- more
Recommanded Articles
This website recommended the use the Chrome browser for journal website.