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Hydro/solvothermal synthesis, crystal structure, and thermal behaviour of piperazine-templated nickel(Ⅱ) and cobalt(Ⅱ)sulfates
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2006, v.19 no.4, pp.309-315
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(2006). Hydro/solvothermal synthesis, crystal structure, and thermal behaviour of piperazine-templated nickel(Ⅱ) and cobalt(Ⅱ)sulfates. Analytical Science and Technology, 19(4), 309-315.
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Abstract
Two piperazine-templated metal sulfate complexes, <TEX>$(C_4N_2H_{12})[Ni(H_2O)_6](SO_4)_2$</TEX>, I and (<TEX>$C_4N_2H_{12}$</TEX>) <TEX>$[Co(H_2O)_6](SO_4)_2$</TEX>, II, have been synthesized by hydro/solvothermal reactions and their crystal structures analyzed by single crystal X-ray diffraction methods. Complex I crystallizes in the monoclinic system, <TEX>$P2_1/n$</TEX> space group, a
- keywords
- Metal(II) sulfate, piperazine, organic template, hydro/solvothermal synthesis, crystal structure, thermal behaviour
Reference
1
Cheetham, A. K, (1999) Angew. Chem. Int. Ed.,
2
Clearfield, A, (1988) Chem. Rev,
3
Alberti, G, (1996) Comprehensive Supramolecular Chemistry, Vol. 7, Chap. 4 & 5, Pergamon Press, New York, U.S.A.
4
Rao, C. N. R, (2004) Angew. Chem. Int. Ed.,
5
Walker, S. M, (1999) J. Am. Chem. Soc.,
6
Conradsson, T, (2000) Inorg. Chem.,
7
Ekambarem, S, (2000) Inorg. Chem.,
8
Choudhury, A, (2002) Angew. Chem. Int. Ed.,
9
Behera, J. N, (2004) Inorg. Chem.,
10
Xing, Y, (2003) J. Chem. Soc. Dalton Trans.,
11
Norquist, A. J, (2002) Chem. Mater.,
12
Khan, M. I, (1999) Inorg. Chim. Acta,
13
Doran, M. B, (2003) Inorg. Chem.,
14
Kim, C. H, (2005) Anal. Sci. & Tech.,
15
Nakamoto, K, (1997) Infrared and Raman Spectra of Inorganic and Coordination Compounds, Part B, John Wiley & Sons, New York, U.S.A.
16
Siemens, (1996) XSCANS Data Collection Package, Siemens, Karlsruhe, Germany
17
Siemens, (1998) SHELXTL Structure Analysis Package, Siemens, Karlsruhe, Germany
18
Sheldrick, G. M, (1990) Acta Cryst.,
19
Paul, G, (2003) Inorg. Chem.,
20
Jayaraman, K, (2002) Solid State Sci.,
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