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- E-ISSN 2288-8985
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Separation properties of 209 PCB congeners on capillary columns and identification of PCBs congeners in aroclor standards for source identification
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2006, v.19 no.4, pp.352-364
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(2006). Separation properties of 209 PCB congeners on capillary columns and identification of PCBs congeners in aroclor standards for source identification. Analytical Science and Technology, 19(4), 352-364.
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Abstract
This study was performed to search for useful separation properties and elution orders of three GC columns (DB-1, DB-5MS, SPB-Octyl) for 209 PCBs congeners using M-1668A-0.01X-SET of the AccuStandard Inc.. In addition, to confirm the quantitative peak in peak pattern method, the IUPAC Nos. of PCBs congener peaks were identified with 4 Aroclor standards (Aroclor-1242, 1248, 1254 and 1260). The separation property of dioxin-like PCBs congeners by four columns (DB-1, DB-5MS, SP-2331 and SPB-Octyl) was excellent in SP-2331. DB-1 and SPB-Octyl columns are necessary to use with a column of other types.
- keywords
- PCBs, GC column, separation property, Aroclor
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