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Analysis of 12 chlorophenols in waste-water using automated liquid phase microextracion (LPME) device
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2007, v.20 no.1, pp.70-77
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(2007). Analysis of 12 chlorophenols in waste-water using automated liquid phase microextracion (LPME) device. Analytical Science and Technology, 20(1), 70-77.
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Abstract
Twelve chlorophenols (CPs) were extracted by liquid phase microextraction (LPME) from the industrial waste-water and analyzed by GC/MS. To establish the optimal conditions, species of extraction solvent, sample amount, pH of sample, salting out effect, a number of sampling and plunger movement speed were investigated. As a result, the linearities of calibaration curves ranged from 0.9913 to 0.9999, while LODs and LOQs were from 0.05 to 10.0 ng/mL except 2,3,4,5-tetrachlorophenol and pentachlorophenol. Using this method, 4-chloro-3-methylphenol confirmed from waste water at the concentration of 784 ng/mL. The method can be applicable to detect chlorophenols from industrial waste-water.
- keywords
- chlorophenols, wastewater, GC/MS
Reference
1
Montero, L, (2005) J. Chromatogr. A,
2
Li, D, (2003) J. Chromatogr. A,
3
Basheer, C, (2004) J. Chromatogr. A,
4
Kee, M. R, (1998) J. Chromatogr. A,
5
Sarrion, M. N, (2003) Rapid Commun. Mass Spectrom.,
6
M. Kawaguchi, (2005) Anal. Chaim. Acta,
7
Rasmussem, K. E, (2004) Trends. Anal. Chem.,
8
Rogers, K. R, (1999) Field analytical chemistry and technology,
9
Zhao, L, (2001) J. Chromatogr. A,
10
Marianna czaplicka, (2003) J. Sep. Sci.,
11
Basheer, C, (2003) J. Chromatogr. A,
12
Jiang, X, (2004) Anal. Chem.,
13
Basheer, C, (2004) J. Chromatogr. A,
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