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Analytical method of the polychlorinated biphenyls in soil using GC/ECD and GC/MS
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2007, v.20 no.2, pp.91-108
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(2007). Analytical method of the polychlorinated biphenyls in soil using GC/ECD and GC/MS. Analytical Science and Technology, 20(2), 91-108.
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Abstract
This study was investigated both the Korean official soil test method and the international various methods for PCBs in soil sample. The analytical guideline of PCBs in contaminated soil were proposed based on the official soil test methods by discussing the extraction, column cleanup, instrumental conditions, quantification methods of peak matching and individual isomers. The total 28 soil samples were selected by consideration of PCBs-contamination, land use etc., and then analyzed using gas chromatography/electron capture detection (GC/ECD) and gas chromatography/mass spectrometry(GC/MS). In this study, the PCBs were not detected as peak matching method using GC/ECD, but PCBs detected <TEX>$0.002{\sim}0.487{\mu}g/kg$</TEX> using GC/MS in background concentrations.
- keywords
- PCBs, Soil, GC/ECD, Aroclor, GC/MS
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