- P-ISSN 1225-0163
- E-ISSN 2288-8985
- Log In/Sign Up
- P-ISSN1225-0163
- E-ISSN2288-8985
- SCOPUS, ESCI, KCI
Article Detail
Home > Article Detail
Characteristics of trace analysis of potential diesel oxygenates using the factorial design in solid-phase microextraction with GC/FID
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2007, v.20 no.5, pp.370-382
&
(2007). Characteristics of trace analysis of potential diesel oxygenates using the factorial design in solid-phase microextraction with GC/FID. Analytical Science and Technology, 20(5), 370-382.
- Downloaded
- Viewed
Abstract
In this study, solid-phase microextraction (SPME) technique using GC/FID was studied as a possible alternative to liquid-liquid extraction for the analysis of EGBE, DGBE, DBM and TGME in water, and an optimization condition of trace analysis of EGBE, DGBE, DBM and TGME using the factorial design was described. Experiments used a fractional factorial design method followed by central composite design allowing optimization of a number of factors as well as statical analysis of results. The response surface analysis showed that the extraction efficiency can be described by a second-order polynomial equation in which the salts concentration, extraction temperature, extraction time and sonication time are the major influences. Using DOE, a new data-dependent method was developed that improved the quantity of confidently analyzed EGBE, DGBE, DBM and TGME in water samples.
- keywords
- SPME, oxygenates, EGBE, DBM, response surface analysis
Reference
1
이규현, (2004) 한국환경분석학회지,
2
안상우, (2004) 한국환경과학회지,
3
조일형, (2006) 대한환경공학회지,
4
조일형, (2007) 한국물환경학회지,
5
박교범, (2000) 분석과학,
6
안상우, (2004) 한국환경분석학회지,
7
김택제, (2002) 분석과학,
8
Marchetti, A, (2003) Chemosphere,
9
Blasco, C, (2004) Journal of Chromatography A,
10
Layton, D. W, (2002) SAE Paper 2002-01-1943,
Other articles from this issue
- Examination about evaluation method of odor active compounds in evaporator by using condensed water
- Characteristics of trace analysis of potential diesel oxygenates using the factorial design in solid-phase microextraction with GC/FID
- Chemical characteristics of PM<sub>2.5</sub> fine particles collected at 1100 site of Mt. Halla during spring seasons between 1998 and 2004
- Development of electrochemical biosensor for determination of galactose
- Comparative analysis of glycerin in cosmetics by LC/MS and <sup>1</sup>H NMR
- Determination of inclusion complex formation constants for the β-CD and [Cu(Dien)(sub-Py)]<sup>2+</sup> ion by the spectrophotometric methods
- Preparation and characterization of CdS nanoparticle on the surface of silica nanoparticles
- Low level tritium analysis using liquid scintillation counter
- Determination of thyroid hormones in plasma samples by high performance liquid chromatograph/diode array detector/electrospray ionization mass spectrometer
- Study on individual characterization of sweat components
- Determination of diallyl disulfide in garlic by reversed-phase high performance liquid chromatography
- Synthesis and structure analysis of the bis(dicyclohexylammonium) chromate dihydrate complex,[(C6H11)2NH2]2[CrO4].2H2O
- more
Recommanded Articles
This website recommended the use the Chrome browser for journal website.