- P-ISSN 1225-0163
- E-ISSN 2288-8985
- P-ISSN1225-0163
- E-ISSN2288-8985
- SCOPUS, ESCI, KCI
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Determination of diallyl disulfide in garlic by reversed-phase high performance liquid chromatography
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2007, v.20 no.5, pp.442-447
Yulia,
P.
, &
(2007). Determination of diallyl disulfide in garlic by reversed-phase high performance liquid chromatography. Analytical Science and Technology, 20(5), 442-447.
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Abstract
The properties of garlic (Allium sativum L.) are attributed to organosulfur compounds. In this paper, an analytical technique with a rapid and simple sample preparation procedures for determination of diallyl disulfide (DADS) in garlic was reported. The DADS was simply extracted with various solvents (methanol, benzene or tetrahydrofuran) from garlic and prepared for HPLC analysis. From the results, the methanol was select as an optimal extraction solvent. The mobile phase was composed from methanol and water, and the gradient elution mode was applied. 0.61 mg of DADS per g garlic powder can be extracted with methanol. This work offers some advantages over the currently accepted techniques and would be useful for chemical and biological studies of garlic and its products.
- keywords
- garlic, dially disulfide, RP-HPLC, extraction
Reference
1
Rahman, K, (2003) Ageing Res. ReV.,
2
Ip, C, (1992) Nutr Cancer,
3
Reddy, B. S, (1993) Cancer Res.,
4
Block, E, (1985) Sci. Am.,
5
Block, E, (1992) Angew Chem. Int. Ed. Eng.,
6
Ueda, Y, (1991) Nippon Shokuhin Kogyo Gakkaishi,
7
Matsuura, H, (1996) Planta Med.,
8
Lawson, L. D, (1991) J. Nat. Prod.,
9
Ziegler, S. J, (1989) Planta Med.,
10
Eckner, M. M, (1992) J. Chromatogr.,
11
Imai, J, (1994) Planta Med.,
12
Krest, I, (2000) J. Agric. Food Chem.,
13
Yoo, K. S, (1998) Sci. Hortic.,
14
Thomas, D. J, (1994) J. Agric. Food Chem.,
15
Ueda, Y, (1990) Agric. Biol. Chem.,
16
Arnault, I, (2003) J. Chromatogr. A,
17
Lawson, L. D, (2005) J. Agric. Food Chem.,
18
Arnault, I, (2005) J. Pharm. Biomed. Anal.,
19
Kubec, R, (1999) J. Chromatogr. A,
20
Lancaster, J. E, (1983) J. Sci. Food Agric.,
21
Keusgen, M, (2003) J. Biosens. Bioelectron.,
22
Synge, R. L. M, (1956) Biochem. J.,
23
Ichikawa, M, (2006) J. Agric. Food Chem.,
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