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  • P-ISSN 1225-0163
  • E-ISSN 2288-8985

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    Synthesis and structure analysis of the bis(dicyclohexylammonium) chromate dihydrate complex,[(C6H11)2NH2]2[CrO4].2H2O

    Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
    2007, v.20 no.5, pp.448-451



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    Abstract

    A new bis(dicyclohexylammonium) chromate dihydrate complex, <TEX>$[(C_6H_{11})_2NH_2]_2[CrO_4]{\cdot}2H_2O$</TEX>, (I), has been synthesized and its structure analyzed by FT-IR, EDS, elemental analysis, ICP-AES, and single crystal X-ray diffraction methods. The Cr(VI) complex (I) is tetragonal system, I<TEX>${\bar{4}}$</TEX>2d space group with a

    keywords
    chromate complex, dicyclohexylammonium ligand, crystal structure, hydrogen bonding


    Reference

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    Bruker, (2001) SMART Data Collection Program, Bruker AXS Inc., Madison, Wisconsin, USA

    2

    Bruker, (2001) SAINT and SADABS Data Reduction and Absorption Correction Program, Bruker AXS Inc.,Madison, Wisconsin, USA

    3

    Bruker, (2001) SHELXTL Structure Analysis Program, Bruker AXS Inc., Madison, Wisconsin, USA

    4

    K. Nakamoto, (1997) Infrared and Raman Spectra of Inorganic and Coordination Compounds, John Wiley & Sons, New York, USA

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