- P-ISSN 1225-0163
- E-ISSN 2288-8985
- Apply for Authority
- P-ISSN1225-0163
- E-ISSN2288-8985
- SCOPUS, ESCI, KCI
Article Detail
Home > Article Detail
Comparison of three analytical methods for PCBs-containing liquid wastes
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2010, v.23 no.3, pp.278-283
https://doi.org/10.5806/AST.2010.23.3.278
&
(2010). Comparison of three analytical methods for PCBs-containing liquid wastes. Analytical Science and Technology, 23(3), 278-283, https://doi.org/10.5806/AST.2010.23.3.278
- Downloaded
- Viewed
Abstract
This study was performed to compare the analytical results among L2000DX and two GC/ECD methods (rapid and conventional). 15 samples of transformer oils were collected to compare the analytical results. In the analytical results of PCBs-containing transformer oil, the PCBs concentrations were in the range of 4.4mg/L to 182.8 mg/L with L2000DX, N.D. to 14.63 mg/L with conventional GC/ECD, and N.D. to 13.03 mg/L using rapid GC/ECD. The PCB concentrations detected with the L2000DX showed a large difference to those detected with GC/ECD methods. Otherwise, little difference was shown between the two GC/ECD methods at a concentration range lower than 4 mg/L, although the rapid GC/ECD method tended to detect a slightly lower concentration near the regulation criteria of Korea for 2 mg/L.
- keywords
- PCBs, GC/ECD, L2000DX, transformer oil
Reference
1
1. UNEP Chemical, “PCB Transformers and Capacitors, From Management to Reclassification and Disposal”, 2002.
2
2. United Nations Environment Programme, “Stockholm Convention on Persistent Organic Pollutants (POPs)” (http://www.pops.int).
3
3. UNEP Chemical, “Regionally based assessment of persistent toxic substances”, Global Report, 2003.
4
4. US EPA, “Guidance on choosing a sampling design for environmental data collection”, EPA/240/R-02/005, 2002.
5
5. M. D. Erickon, “Analytical Chemistry of PCBs”, Lewis Publishers, New York, 1997.
6
6. V. den Berg, M. Birnbaum and A. Bosabel, Environ. Health Persp., 106(12), 775-792(1998).
7
7. 국립환경연구원, “폴리염화비페닐류(PCBs) 함유 폐기물의 적정관리방안에 관한 연구”, 2003.
8
8. 국립환경과학원, “PCBs 업무편람”, 2008.
9
9. 환경부, “PCBs 함유 폐기물 간이방법 적용 및 운영지침”, 2007.
10
10. 환경부, “폐기물관리법”.
11
11. L2000DX User's Manual Version 1.24 Rev 4. (http://www.dexsil.com), 2006.
12
12. 환경부, “폐기물공정시험방법”, 2008.
13
13. S. K Shin, T. W. Jeon, J. K. Yoon, T. S. Kim, G. J. Oh, Y. S. Kim and K. S. Kim, Anal. Sci. Technol. 21(3), 174-182(2008).
Other articles from this issue
- Characterization of Fe-ACF/TiO2 composite and photocatalytic activity for MB Solution under visible light
- Fabrication of ordered porous nanocomposite materials using templating
- Determination and preconcentration of Cu(II) using microcrystalline p-Dichlorobenzene loaded with salicylaldoxime
- Estimation on the application of Reference Materials for PCBs Proficiency Testing from the transformer oil
- The TVOC management level evaluation of adhesive product following to simultaneous revision of indoor air quality testing methods and standards
- Assessment of PCBs-containing solid wastes using official wastes test method
- Distribution and emission source of PAHs in ambient air of Seoul
- Comparison of three analytical methods for PCBs-containing liquid wastes
- Evaluation of the proficiency testing results using river water-based reference materials for heavy metal analysis
- Preparation of wastewater-based reference materials for heavy metal analysis and interlaboratory study
- The study of nondestructive evaluation method of paper records materials by NIR spectroscopy
- Distribution and exposure assessment of indicator PCBs in Food
- Analysis of rifle and pistol primer gunshot residue using SEM-EDX
- more
Recommanded Articles
This website recommended the use the Chrome browser for journal website.