- P-ISSN 1225-0163
- E-ISSN 2288-8985
- Log In/Sign Up
- P-ISSN1225-0163
- E-ISSN2288-8985
- SCOPUS, ESCI, KCI
Article Detail
Home > Article Detail
Gas chromatographic profiles of rose essential oils: a round-robin test on oil of rose, Chinese Kushui type (Rosa sertata × Rosa rugosa)
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2012, v.25 no.4, pp.207-213
https://doi.org/10.5806/AST.2012.25.4.207
&
(2012). Gas chromatographic profiles of rose essential oils: a round-robin test on oil of rose, Chinese Kushui type (Rosa sertata × Rosa rugosa). Analytical Science and Technology, 25(4), 207-213, https://doi.org/10.5806/AST.2012.25.4.207
- Downloaded
- Viewed
Abstract
Analysis of the aroma constituents present in the rose essential oil of Chinese Kushui type (Rosa sertata × Rosa rugosa) by GC-FID and GC-MS was performed independently as an expert for the inter-laboratory round-robin test to verify reproducibility according to the decision of the preliminary meeting of ISO/TC-54(Shanghai, Sep. 14-15, 2010). Total 179 peaks (using SPB-1 apolar column), 165 peaks (using DB-624 intermediate polar column), and 162 peaks (using Supelcowax-10 polar column) were separated by GC-FID, respectively. Major constituents (over 5%) by GC-FID were β-citronellol (41.6~46.7%), geraniol (9.7~11.0%), and nerol (3.4~4.5%). β-Citronellol peak was overlapped with nerol peak on SPB-1 and DB-624 columns, whereas the two peaks were separated each other on Supelcowax-10 column. Our results were generally consistent with Chinese data (ISO/DIS 25175); however, a peak of phenethyl alcohol separated by using PEG (Supelco wax)column was found at the quite different retention time. Comparative analysis was conducted using Bulgarian rose (Rosa damascena Miller) oil and perfume. Bulgarian rose oil showed rich amounts of characteristic aroma constituents than the essential oil of Chinese Kushui type.
- keywords
- GC-FID, GC/MS, rose essential oils, chinese kushui type, aroma, round robin test for ISO/TC-54
Reference
1
1. A. V Roberts, T. Debener, S. Gudin edt., Encyclopedia of Rose Science, Vol. 1, pp. 387-414, Elsevier Academic Press, Oxford, UK, 2003.
2
2. X. S. Zhou, Y. M. Jiang, Y. Bi, J. X. Li, Z. G. Qi and S. H. Zhang, Sci. Technol. Food Ind., (in Chinese), 30(11), 226-228 (2009).
3
3. K. E. Rusanov, N. M. Kovacheva and I. I. Atanassov, Biotechnol. Biotec. EQ. 25, 2210-2216 (2011).
4
4. A. Almsirad, Y. Amanzadeh, A. Taheri and M. Iranshahi, J. Essent. Oil Res., 19, 110-112 (2007).
5
5. A. Moustafavi and D. Afzali, Chem. Nat. Compd., 45(1), 110-113 (2009).
6
6. H. Longhmani-Khouzani and O. Sabzi Fini, J. Safari, Sci. Iran., 14(4), 316-319 (2007).
7
7. W. Zhou, Y. H. Zhang, H. L. Xu and M. Gu, Rapid Commun. Mass Spectrom., 25(20), 3097-3102 (2011).
8
8. W. Zhou, X. P. Zhou, G. H. Zhao, H. W, Liu, L. Ding and L. R. Chen, Chin. J. Chromatogr., (in Chinese), 20(6), 561-564 ( 2002).
9
9. L. G. Feng, L. X. Sheng, L. Y. Zhao, X. Y. Yu, D. W. Shao and X. D. He, Sci. Agric. Sin., (in Chinese), 41 (12), 4341-4351 (2008).
10
10. H. J. Kim, K. Kim, N. S. Kim and D. S. Lee, J. Chromatogr. A, 902, 389-404 (2000).
11
11. M. M. Won, E. J. Cha, O. K. Yoon, N. S. Kim, K. Kim and D. S. Lee, Anal. Chim. Acta, 631, 54-61 (2009).
12
12. D. S. Lee, M. M. Won and M. S. Chun, J. Natural Science, (Seoul Women’s Univ. in Korean), 20, 103-106 (2008).
13
13. ISO 9842:2003(E) Oil of rose (Rosa × damascena Miller).
14
14. J. Lawless, Encyclopedia of Essential Oils: The Complete Guide to The Use of Aromatic Oils In Aromatherapy, Herbalism, Health and Well Being, Thorsons Publisher, London, UK, 2002.
15
15. W. G. Taylor and C. E. Schreck, J. Pharm. Sci., 74(5), 534-539 (1985).
Other articles from this issue
- Gas chromatographic profiles of rose essential oils: a round-robin test on oil of rose, Chinese Kushui type (Rosa sertata × Rosa rugosa)
- Analysis of biodiesel quality based on infrared spectroscopy and multivariate statistics
- Signal compensation by the light scattering of sample aerosols in ICP-AES
- The study of quantitative analysis for noxious gases of plastic materials by remote sensing open path FT-IR spectrometer
- Determination of hazardous semi-volatile organic compounds in industrial wastewater using disk-type solid-phase extraction and GC-MS
- Study on distribution characteristics of brominated flame retardants in sediments
- Establishment of content criteria of marker compounds through the monitoring of Achyranthis Radix collected from Korea and China
- Residue analysis of penicillines in livestock and marine products
- more
Recommanded Articles
This website recommended the use the Chrome browser for journal website.