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- E-ISSN 2288-8985
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Analysis of E,E-farnesol and squalene in makgeolli using stir bar sorptive extraction coupled with gas chromatography-mass spectrometry
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2014, v.27 no.1, pp.60-65
https://doi.org/10.5806/AST.2014.27.1.60
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(2014). Analysis of E,E-farnesol and squalene in makgeolli using stir bar sorptive extraction coupled with gas chromatography-mass spectrometry. Analytical Science and Technology, 27(1), 60-65, https://doi.org/10.5806/AST.2014.27.1.60
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Abstract
The aim of this study was to establish an analytical method for the determination of E,E-farnesoland squalene in makgeolli, which is a traditional type of Korean fermented rice wine. E,E-farnesol and squalenein makgeolli were extracted using stir bar sorptive extraction (SBSE) coupled with gas chromatography-massspectrometry. SBSE was found to be an effective method for analyzing the E,E-farnesol and squalene levelsin makgeolli. The linear dynamic range of the SBSE method for detecting E,E-farnesol and squalene rangedfrom 0.5 to 200 ng/mL with R2=0.9974 for E,E-farnesol and 100 to 50000 ng/mL with R2=0.9982 for squalene. The limit of detection and the limit of quantification using the SBSE method were 0.1 and 0.5 ng/mL for E,Efarnesoland 15.0 and 40.0 ng/mL for squalene, respectively. The average recoveries obtained were, quantitatively,101-107% for E,E-farnesol and 98-103% for squalene, respectively, supporting the accuracy of the SBSE-GCMSmethod.
- keywords
- makgeolli, E, E-farnesol, squalene, SBSE-GCMS
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