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- E-ISSN 2288-8985
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- P-ISSN1225-0163
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Spectroscopic Studies on Crystallization of Na, TPA-ZSM-5 synthesized at Low Temperature and Atomospheric pressure
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
1997, v.10 no.1, pp.18-30
Yun,
Y. J., &
Ha,
J.
M.
(1997). Spectroscopic Studies on Crystallization of Na, TPA-ZSM-5 synthesized at Low Temperature and Atomospheric pressure. Analytical Science and Technology, 10(1), 18-30.
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Abstract
Na, TPA-ZSM-5 with Si / Al mole ratio of about 130 was synthesized at low temperature and atmospheric pressure. These intermediate products were characterized by using XRD, XRF, FT-IR, NMR, and SEM. As a result, intermediate product were different from those that synthesized by autoclave method but spectroscopic characteristics of the final products showed to be in the typical ZSM-5 region. The defect sites were observed in the final product and removed by calcination at <TEX>$540^{\circ}C$</TEX>. Na, TPA-ZSM-5, aboveall, was synthesized at this condition within 48hr.
- keywords
- synthesized at low temperature and atmospheric pressure, defect sites
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