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Analysis of Nitrophenols Using Liquid Chromatography/Atmospheric Pressure Chemical Ionization Mass Spectrometry
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
1997, v.10 no.1, pp.9-17
Hong,
J., Yoo,
J. S., &
Kim,
K.
(1997). Analysis of Nitrophenols Using Liquid Chromatography/Atmospheric Pressure Chemical Ionization Mass Spectrometry. Analytical Science and Technology, 10(1), 9-17.
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Abstract
Nitrophenols are a group of important priority pollutants classified by the US Environmental Protection Agency. Reverse-phase liquid chromatographic method combined with mass spectromethy employing atmospheric pressure chemical ionization(APCI) interface is utilized to determine a mixture of nitrophenols in water matrix without any pretreatment. The sensitivity and selectivity for the identification of different kind of nitrophenols is enhanced by the use of selected ion monitoring and cone voltage fragmentation. The fragmentation patterns of nitrophenols are compared with those obtained from the collision induced dissociation(CID) MS/MS technique.
- keywords
- nitrophellols, LC/MS, APCI, cone voltage fragmentation
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