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<TEX>$({\eta}^5-C_5Me_5)_2BiCl$</TEX>, The First Organobismuth Compound with <TEX>$\pi$</TEX>-bonded Cyclopentadienyl Ring Analysized by X-ray Diffractometry
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
1998, v.11 no.1, pp.42-46
Lorberth,
J., Shin,
S., &
Kong,
Y.
K.
(1998). <TEX>$({\eta}^5-C_5Me_5)_2BiCl$</TEX>, The First Organobismuth Compound with <TEX>$\pi$</TEX>-bonded Cyclopentadienyl Ring Analysized by X-ray Diffractometry. Analytical Science and Technology, 11(1), 42-46.
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Abstract
The reaction of <TEX>$({\eta}^5-C_5Me_5)_2K$</TEX> with <TEX>$BiCl_3$</TEX> yielded <TEX>$({\eta}^5-C_5Me_5)_2BiCl$</TEX>[I], the first organobismuth compound with <TEX>${\pi}$</TEX>-bonded cyclopentadienyl ring. The compound I which was the violet crystal (yield, 30%) was decomposed to <TEX>$PCpBiCl_2$</TEX>. The Structure of <TEX>$({\eta}^5-C_5Me_5)_2BiCl$</TEX> was identified as single crystal by X-ray diffraction method. The eliminated product <TEX>$C_{20}H_{30}$</TEX>, triclinic crystal of space group p1(Z
- keywords
- bis (pentamethylcyclopentadienyl) bismuth, single crystal X-ray crystallography, organobismuth compound
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