- P-ISSN 1225-0163
- E-ISSN 2288-8985
- Log In/Sign Up
- P-ISSN1225-0163
- E-ISSN2288-8985
- SCOPUS, ESCI, KCI
Article Detail
Home > Article Detail
Thermal Stability and Deintercalation of K-synthetic Graphite Intercalation Compounds at Elevated Temperatures
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
1998, v.11 no.2, pp.92-95
Oh,
W., Lee,
Y., &
Ko,
Y.
(1998). Thermal Stability and Deintercalation of K-synthetic Graphite Intercalation Compounds at Elevated Temperatures. Analytical Science and Technology, 11(2), 92-95.
- Downloaded
- Viewed
Abstract
K-SGICs(synthetic graphite intercalation compounds) were synthesized in a modified two-bulb pyrex tube. The pressure in the two-bulb tube was maintained at approximately <TEX>$10^{-3}$</TEX> torr for the reaction of potassium and graphite. Deintercalation process of the K-SGlCs obtained by the modified method was heat-treated by keeping in liquid paraffin between <TEX>$25^{\circ}C$</TEX> and <TEX>$1400^{\circ}C$</TEX>. The thermal stability and the temperature dependence of the K-SGICs were characterized using differential scanning calorimeter(DSC) analyzer. Enthalpy and entropy for K-SGIC formations were calculated by confirming the deintercalation and thermodynamic exothermic reactions depending on the various temperatures. The structure changes and thermal stability of K-SGICs during the deintercalation reaction of potassium ions and the interlayer spaces of the synthetic graphite were identified by X-ray diffraction(XRD).
- keywords
- Potassium, Synthetic graphite, Deintercalation, Stability, Enthalpy and entropy, DSC, XRD
- Downloaded
- Viewed
- 0KCI Citations
- 0WOS Citations
Other articles from this issue
- SPF Measurement and Cytotoxicity of Sunscreen Agents in Cosmetic
- Bromide Concentration in Human Biological Samples Intoxicated by Methylbromide
- Thermal Stability and Deintercalation of K-synthetic Graphite Intercalation Compounds at Elevated Temperatures
- Development of a Multi - channel Detector for Capillary Electrophoresis System
- The Study on the Biodegradability and Phosphate, Heavy Metal Contents of Shampoos and Powder Detergents for Clothing
- The Study of Fast X-ray Fluorescence Analysis Using a SSQ Program
- Determination of Germanium in Spring Waters by Inductively Coupled Plasma Mass Spectrometry
- Tarnish Behavior of Palladium-Indium-Silver alloy
- Analysis of Polyamine Transport of Young Spring Radish Cotyledons
- Analysis of the Change of Amino Acids by Cadmium and Polyamine-Treatment in Spring Radish Young Cotyledons and Roots
- Simple Analytical Method for Acrylamide in the Workplace Air Adsorbed by Charcoal Tube
- Stability Constants for Co(II) and Zn(II) of Multidentate N,O-Schiff Base Ligands in Dioxane-Water Mixtures
- Forensic Analysis of Human DNA
- more
Recommanded Articles
This website recommended the use the Chrome browser for journal website.