- P-ISSN 1225-0163
- E-ISSN 2288-8985
- Apply for Authority
- P-ISSN1225-0163
- E-ISSN2288-8985
- SCOPUS, ESCI, KCI
Article Detail
Home > Article Detail
A Study of Analytical Method for Trace Metal Ions in Whole Blood and Urine by Inductively Coupled Plasma-Mass Spectrometry using Solid-Liquid Extraction Technique
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
1998, v.11 no.4, pp.281-291
Lee,
W., Hur,
Y., &
Park,
K.
(1998). A Study of Analytical Method for Trace Metal Ions in Whole Blood and Urine by Inductively Coupled Plasma-Mass Spectrometry using Solid-Liquid Extraction Technique. Analytical Science and Technology, 11(4), 281-291.
- Downloaded
- Viewed
Abstract
An analytical method for the simultaneous measurement of trace Cu, Sn, and Bi in blood and urine has been investigated by Inductively Coupled Plasma-Mass Spectrometry (ICP-MS). Microwave oven was used for the pretreatment of blood samples using nitric acid and hydrogen peroxide in a closedvessel digestion system with 1 mL whole blood for 8 minutes. Amberlite IRC-718 resin was used as a solid phase in solid-liquid extraction technique for the removal of matrix interferences such as Na, S, P, and other polyatomic ion species. Detection limits for Cu, Sn, and Bi by this method were 0.000375 ng/mL, 0.000297 ng/mL, and 0.000174 ng/mL, respectively. Recoveries of 99.1% for Cu, 102.5% for Sn, and 98.4% for Bi were obtained for the standard spiked NIST SRM 955a blood sample. The developed method was applied for whole real blood and urine samples.
- keywords
- lCP-MS, whole blood, urine, analysis, solid-liquid extraction
- Downloaded
- Viewed
- 0KCI Citations
- 0WOS Citations
Other articles from this issue
- Enrichment of Lithium Isotope by Novel Ion Exchanger Containing Azacrown Ether as Anchor Group
- Potentiometric Response of Chitin - based Membrane Electrode to various Metal cations
- The Development of Cisplatin Analysis Method in Plasma by Flameless Atomic Absorption Spectrometry
- Adsorption and Separation Behaviors of Metal Ions Using a Poly-Dibenzo-18-Crown-6 in Aqueous Solution
- Adsorption Characteristics of Cr(VI) on the Oak Sawdust
- Effect of Supporting Anions on Particle Characteristics of Barium Titanyl Oxalate Formed by Homogeneous Precipitation
- Adsorption and Antibacterial Properties of Metal Treated Activated Carbon
- Preparation and Certification of Rice Flour Reference Materials for Trace Elements Analysis
- A Study of Analytical Method for Trace Metal Ions in Whole Blood and Urine by Inductively Coupled Plasma-Mass Spectrometry using Solid-Liquid Extraction Technique
- Separation of Functionalized Heterocyclic Compounds by High Performance Liquid Chromatography (II)
- Matrix effect on the Determination of Inorganic Priority Pollutants in Sludges
- An Optochemical Sensor for the Determination of Divalent Transition Metal Ions Based on a Reactive Dye
- Analysis of Ultra Pure Sulfuric Acid for Semiconductor Using High Resolution ICP-MS
- Characterization of Ferrous Metal Artifacts by Microstructure Observation
- Characterization of Semiconductor Using Neutron Activation Analysis-I (Its Principle and Wafer Bulk Analysis)
- more
Recommanded Articles
This website recommended the use the Chrome browser for journal website.