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Quantitative Analysis of Trace Metals in Lithium Molten Salt by ICP-AES
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2000, v.13 no.3, pp.309-314
Kim,
D., Pyo,
H., Park,
Y., Park,
Y., &
Kim,
W.
(2000). Quantitative Analysis of Trace Metals in Lithium Molten Salt by ICP-AES. Analytical Science and Technology, 13(3), 309-314.
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Abstract
The quantitative analysis of various trace metals including fission products in lithium molten salts has been performed using a inductively coupled plasma atomic emission spectrometer (ICP-AES). The spectral interferences of lithium content, 500, 1,000 and 2,000 mg/L, in the sample solution were investigated using an optimum wavelength for the respective metal species. As a result, the line intensities for Y, Nd, Sr, and La had no influences from the lithium content up to 2,000 mg/L, while Mo, Ba, Ru, Pd, Rh, Zr and Ce showed spectral interferences of 10% to 50%. The group separation of metals from lithium in the molten salts solution was carried out by adding ammonia water into the solution. The recovery of Ru, Y, Rh, Zr, Nd, Ce, La and Eu was found to be over 90%, while Mo, Ba, Pd, and Sr provided low recovery percentages.
- keywords
- Lithium molten salt, ICP-AES, Analysis of fission product, Group separation
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