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  • P-ISSN 1225-0163
  • E-ISSN 2288-8985

Synthesis and Characterization of Intercalation Compounds of Alkylsulfonate into Hydrated and Dehydrated Zinc

Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2000, v.13 no.3, pp.338-345
Huh, Young Duk
Park, Sung Hun
Jun, Tae Hyun
Park, Yong Jun
Park, Yang Sun
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Abstract

The intercalated compounds of alkylsulfonate into hydrated and dehydrated zinc were synthesized. From the XRD, FT-IR, TGA, elemental analysis data, and the molecular size, the orientation of the intercalated alkylsulfonates was determined. For the hydrated compounds, alkylsulfonates were intercalated into hexaqua zinc layer with the bilayer structure of <TEX>$32.9^{\circ}$</TEX> angle of inclination. For the dehydrated compounds, alkylsulfonates were directly bonded to zinc ion with the bilayer structure of <TEX>$51.4^{\circ}$</TEX> angle of inclination.

keywords
Alkylsulfonate, Intercalation, Layered structure


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