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- E-ISSN 2288-8985
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Characteristic Feature of Inductively Coupled Plasma Atomic Emission Spectrometer/Shielding System and Evaluation of Its Applicability to Analysis of Radioactive Materials
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2000, v.13 no.4, pp.474-483
Lee,
C. H., Suh,
M. Y., Choi,
K. C., Park,
Y. S., Jee,
K. Y., &
Kim,
W.
H.
(2000). Characteristic Feature of Inductively Coupled Plasma Atomic Emission Spectrometer/Shielding System and Evaluation of Its Applicability to Analysis of Radioactive Materials. Analytical Science and Technology, 13(4), 474-483.
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Abstract
An inductively coupled plasma atomic emission spectrometer/shielding system was specially designed and built for the analysis of radioactive materials. Both of an inductively coupled plasma source and a sample transfer system to be contacted with radioactive materials was installed in a stainless steel glove box. In terms of analytical capability and radiation safety, characteristic feature of the system was investigated. Its applicability to the determination of fission products and corrosion products in the radioactive materials such as spent fuel dissolver solution and the primary coolant of nuclear power reactors was evaluated. In the concentration range <TEX>$0.01-0.1mgL^{-1}$</TEX>, the relative standard deviation was found to be less than 5%.
- keywords
- ICP-AES, glove box, radioactive materials, fission products, corrosion products
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