- P-ISSN 1225-0163
- E-ISSN 2288-8985
- P-ISSN1225-0163
- E-ISSN2288-8985
- SCOPUS, ESCI, KCI
Article Detail
Home > Article Detail
Method for the Analysis of Polybrominated Biphenyls(PBBs) in Environmental Samples
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2002, v.15 no.3, pp.14-316
&
(2002). Method for the Analysis of Polybrominated Biphenyls(PBBs) in Environmental Samples. Analytical Science and Technology, 15(3), 14-316.
- Downloaded
- Viewed
Abstract
extraction methods of PBBs from environmental samples by soxhlet extraction for solid phase and liquid-liquid extraction for liquid phase were compared. After extraction, silicagel and florisil as column clean up methods were used for the comparison of cleanup efficiency with different solvent system. Also, the analytical instruments were used GC/MSD.The 22 kinds of PBBs standards were used to establish the analytical methods to perform the experiments of recoveries and detection limits in water and soil. The detection limits of PBBs represented 5∼10 ng/L for water and 0.5∼3.5 ng/g for soil samples, respectively. The recoveries of water samples represented 96∼107% in n-hexane, dichloromethane and toluene for water, and 60∼80% in combined solvent with n-hexane and acetone. The recoveries of soil sample were surveyed 67∼97% in soxhlet extraction and 64∼76% in ultrasonic extraction with selected solvents.
- keywords
- brominated flame retardants(BFRs), polybrominated biphenyls(PBBs)
Other articles from this issue
- Analysis of Cyclofenil and its Metabolites in Human Urine using GC/MS
- Mutation Analysis in β2-Adrenergic Receptor Gene by Denaturing High Performance Liquid Chromatography (DHPLC)
- Comparison of isoButoxycarbonyl derivatives, tert.-butyldimethylsilyl derivatives, with US EPA Method in the sensitivity of Alkylphenols, Chlorophenols, and Bisphenol A Potential field-screening applications of GC/MS-SIM
- Adsorptive Catalytic Wave of Chromium-Cupferron Complex
- Analysis of derivatized MX by Gas Chromatography/Mass Spectrometry
- Wettability and Aging Effect of Polystyrene Film Treated by PSII according to the Molecular Weight
- The Studies of Conductive and Non-Conductive Multi-Layer Depth Analysis by Radio Frequency Gas-Jet Boosted Glow Discharge Atomic Emission Spectrometry
- Determination of Diazepam in Intact Diazepam Tablets Using Near Infrared Spectroscopy
- Liquid chromatographic determination of α-, β-, γ-, and δ-tocopherol in sesame oils of different origin
- Simultaneous Removal of NOx/SOx by Catalyst-loaded Cordierite Porous Filter
- A Study on the Characteristics of VOC Removal by Cordierite Filter Loaded with Catalyst
- Residue and Risk Assessment of Polychlorinated dibenzo-p-dioxin/dibenzofurans in the Korean Population
- The Distributions of PCBs in Inchon Coastal Sediments
- Method for the Analysis of Polybrominated Biphenyls(PBBs) in Environmental Samples
- Synthesis and Structural Analysis of the Diaquabis(ethylenediamine)nickel(II) Bis(p-toluenesulfonate) Monohydrate
- Mutation Analysis in β<sub>2</sub>-Adrenergic Receptor Gene by Denaturing High Performance Liquid Chromatography (DHPLC)
- Liquid chromatographic determination of α-, β-, γ-, and δ-tocopherol in sesame oils of different origin
- more
Recommanded Articles
This website recommended the use the Chrome browser for journal website.