- P-ISSN 1225-0163
- E-ISSN 2288-8985
- Apply for Authority
- P-ISSN1225-0163
- E-ISSN2288-8985
- SCOPUS, ESCI, KCI
Article Detail
Home > Article Detail
Reaction morphology depending on the amounts of HCl and NH<sub>4</sub>OH and effect of pH on the preparation of TiO<sub>2</sub> nanopowder
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2007, v.20 no.4, pp.302-307
&
(2007). Reaction morphology depending on the amounts of HCl and NH<sub>4</sub>OH and effect of pH on the preparation of TiO<sub>2</sub> nanopowder. Analytical Science and Technology, 20(4), 302-307.
- Downloaded
- Viewed
Abstract
The reaction morphology was investigated depending on the amounts of HCl and <TEX>$NH_4OH$</TEX>, and the effect of pH was studied on the preparation of <TEX>$TiO_2$</TEX> nanopowders. <TEX>$TiO_2$</TEX> nanopowder was prepared using a titanium tetra-isopropoxide. Subsequently, the effect of pH on the characteristics of the prepared <TEX>$TiO_2$</TEX> nanopowder was evaluated depending on the amounts of the catalysts such as HCl and <TEX>$NH_4OH$</TEX>. The morphology and phase transformation of <TEX>$TiO_2$</TEX> powder prepared by hydrolysis of titanium tetra-isopropoxide were strongly influenced by the presence of the catalysts. In the case of using <TEX>$NH_4OH$</TEX>, the morphology of the <TEX>$TiO_2$</TEX> powder exhibited powder form. For the HCl catalyst, it showed bulk or granule form. The phase transformations of amorphous <TEX>$Ti(OH)_4$</TEX> to anatase <TEX>$TiO_2$</TEX> and the anatase to rutile was significantly influenced by the kind and amount of thecatalysts.
- keywords
- Reaction morphology, <TEX>$TiO_2$</TEX> nanopowder, catalyst, pH
Reference
1
Tai, (1993) Proceedings of ISES Solar World Congress Budapest,
Other articles from this issue
- Tightness of specimen sealing box in 20 L test chamber to evaluate building materials emitting pollutants
- Survey of nitroso-compounds level derived from additives in metal-working fluids
- The analysis for the HCl modification effect and formation of TiO<sub>2</sub> on activated carbon fiber surface
- Voltammetric measurements of iron using an infrared photodiode electrode
- Surface analysis of rayon-based carbon nanofibers and activated carbon fibers
- Reaction morphology depending on the amounts of HCl and NH<sub>4</sub>OH and effect of pH on the preparation of TiO<sub>2</sub> nanopowder
- Simultaneous determinations of anthracycline antibiotics by high performance liquid chromatography coupled with radial-flow electrochemical cell
- Determination of pseudoephodrine, dextromethorphan and their metabolites in human urine by gas chromatography - mass spectrometry
- Development of a rapid HPLC method for the determination of penciclovir in human plasma using a monolithic column and its application to a bioequivalence study
- Qunatitative analysis of liquiritin and glycyrrhizin in glycyrrhizae radix by HPLC-MS/MS
- Molecular holographic QSPR analysis on the reactivity between glycine and ninhydrin analogues as latent fingerprints detector
- Determination of residual novobiocin in livestock products and fisheries products by HPLC
- Structural characterization of ladder-type cadmium(Ⅱ) citrate complex, (C3H12N2)[{Cd(H2O)(C6H5O7)}2],6H2O
- more
Recommanded Articles
This website recommended the use the Chrome browser for journal website.