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Analysis of ethyl carbamate in alcoholic beverages
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2008, v.21 no.1, pp.53-57
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(2008). Analysis of ethyl carbamate in alcoholic beverages. Analytical Science and Technology, 21(1), 53-57.
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Abstract
주류 중 에틸카바메이트의 함량을 조사하기 위해 시중에 유통되는 시료를 고체상 정제컬럼(충 진제: 규조토)에 흡착시켜 디클로로메탄으로 용출시킨 후 GC/MS-SIM 방법에 의해 분석하였다. 적용된 분석법의 회수율은 85.2-87.9% 이었으며 변이계수는 0.7-1.9%, 검출한계는 2 μg/kg, 정량한계는 10 μg/ kg이었다. 에틸카바메이트의 함량을 조사한 결과는 대상 주류의 유형에 따라 검출수준에 차이를 나타냈 으며, 평균 검출수준은 리큐르 194 μg/kg, 과실주 105 μg/kg, 일반증류주 62 μg/kg, 청주 28 μg/kg, 약주 15 μg/kg, 기타 주류 12 μg/kg, 소주 불검출 이었다.
- keywords
- ethyl carbamate, alcoholic beverages, GC/MS
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