- P-ISSN 1225-0163
- E-ISSN 2288-8985
- P-ISSN1225-0163
- E-ISSN2288-8985
- SCOPUS, ESCI, KCI
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Determination of residual flumethrin in honey products by HPLC
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2009, v.22 no.6, pp.458-463
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(2009). Determination of residual flumethrin in honey products by HPLC. Analytical Science and Technology, 22(6), 458-463.
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Abstract
A new quantitative analytical method has been established for the rapid determination of flumethrin in honey products using high performance liquid chromatography (HPLC). Sample was dissolved and extracted in the mixture of water and acetonitrile (1:2). The extracts were purified with silica cartridge eluted by the mixture of hexane and dichloromethane (55:45) and analyzed at 266 ㎚ using HPLC. The percentage recovery of flumethrin spiked in sample was found to be 90.2-97.8% and the limit of detection is 0.003 ㎎/㎏. We validated the method for the linearity, the precision and the reproducibility. We investigated the residues of flumethrin in honey products retailed in market using the established method. Flumethrin was not detected at all among 130 samples of honey.
- keywords
- flumethrin, honey, mite, acaricide, HPLC
Reference
1
1. 김병호외 11명, ‘최신 양봉학’, 1996년판, 270-280, 선진문화사, 1996.
2
2. 농축산기술자원연구소, 양봉 새 기술, 2007년판, 250-253, 내외출판사, 2002.
3
3. 정진교, 이만영, 마영일, 한국양봉학회지, 15(2), 141-145(2000).
4
4. 이명렬, 최지영, 이만영, 김영수, 한국양봉학회지,18(2), 151-154(2003).
5
5. 최승윤, ‘양봉 꿀벌과 벌통’, 2004년판, 252-280, 오성출판사, 2004.
6
6. F. Mutinelli, APIACTA, 38, 149-155(2003).
7
7. 조도행, ‘양봉 사계절 관리법’, 2006년판, 30-36, 오성출판사, 2006.
8
8. 이명렬, 이만영, 김영수, 남성희, 장승종, 유철형, 한국양봉학회지, 19(1), 57-60(2003).
9
9. S. Frison, W. Breitkreitz, R. Currie, D. Nelson, P. Sporns, Food Research International, 32, 35-41(1999).
10
10. H. I. Assil, P. Sporns, Journal of Agricultural and Food Chemistry, 39, 2206-2213(1991).
11
11. R. Rial-Otero, E.M. Gaspar, I. Moura, J.L. Capelo, Talanta, 71, 1906-1914(2007).
12
12. 식품공전, 식품의약품안전청, 2007.
13
13. A. Kamel, A. Al-Ghamdi, Journal of Environmental Science and Health Part B, 41, 159-165(2006).
14
14. S. Adamczyk, R. Lazare, A. Herrera, Analytica Chemica Acta, 581, 95-101 (2007).
15
15. J. J. Jimennez, J. L. Bernal, M. J. del Nozal, C. Alonso, Journal of Chromatography A, 1048, 89-97(2004).
16
16. Validation Guidelines, Codex Committee on Residues of Veterinary Drugs in Food, 11th Session (1998).
17
17. E. Korta, A. Bakkali, L. A. Berrueta, B. Gallo, F. Vicente, Journal of Chromatography A, 930, 21-29 (2001).
18
18. The Horticulture & Food Research Institute of New Zealand Ltd, Apicata, 1-33(2003).
19
19. S. Bogdanov, V. Kilchenmann, A. Imdorf, Swiss Bee Research Center Report (1999).
20
20. 한국동물용의약품협회 DB 자료 (KAHPA, http://kapha.or.kr/indx_k.htm), 2005.
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