• P-ISSN1225-0163
  • E-ISSN2288-8985
  • SCOPUS, ESCI, KCI

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  • P-ISSN 1225-0163
  • E-ISSN 2288-8985

A identification of sprayed fire-resistive materials by near-infrared spectroscopy

Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2011, v.24 no.2, pp.85-93
https://doi.org/10.5806/AST.2011.24.2.085






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Abstract

To protect the steel structure in a high story buildings from fire, the sprayed fire-resistive materials are applied during the construction. Current standard methods to check the quality of sprayed fire-resistive materials are real fire test in lab, which take a long time (several weeks) and expensive. In this study, a simple analytical method to check the quality of sprayed fire-resistive materials is developed using Near Infrared Spectroscopy (NIR). Total 9 kinds of sprayed fire-resisted materials and 3 kinds of normal sprayed material sets were used for the analysis. Each set of materials was 50 to 100 samples. Samples are grinded and make a fine powder. The spectral data acquisition was carried out using FT-NIR spectrometer with a integrating sphere. NIR methods successfully identify the sprayed fire resistive materials by a principle component analysis (PCA)after a vector normalization (SNV) pretreatment.

keywords
NIR spectrometer, FT-NIR, Fire-resistive materials, PCA


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