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The rapid determination of PAHs in foods using ultra high performance liquid chromatography
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2011, v.24 no.4, pp.266-274
https://doi.org/10.5806/AST.2011.24.4.266
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(2011). The rapid determination of PAHs in foods using ultra high performance liquid chromatography. Analytical Science and Technology, 24(4), 266-274, https://doi.org/10.5806/AST.2011.24.4.266
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Abstract
Using a Hitachi LaChrom Ultra 2000U, a reverse phase ultra high performance liquid chromatography (u-HPLC) method was developed for the rapid quantification of 14 PAHs in foods. The proposed method for PAH analysis is based on solid phase extraction (SPE) cartridges; the determination was carried out by u-HPLC with fluorimetric detection. The method was very sensitive; PAH concentration levels were in a low μg/kg range and could be detected and quantified. Six samples of food were analyzed. Among PAHs, PHE was found in most of samples, the concentration ranging from 2.5 to 19.9 μg/kg. The contents of benzo[c]fluorine (BCL),pyrene (PYR), benzo[a]anthracene (BaA), chrysene (CHR), benzo[b]fluoranthene (BbF), benzo[k]fluoranthene (BkF) were low at the ‘μg/kg’ level or were less than LOD.
- keywords
- UHPLC, rapid analysis, PAHs
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