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- E-ISSN 2288-8985
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Quality inspections of active components in oxidative hair coloring products by UPLC
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2013, v.26 no.1, pp.99-105
https://doi.org/10.5806/AST.2013.26.1.099
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(2013). Quality inspections of active components in oxidative hair coloring products by UPLC. Analytical Science and Technology, 26(1), 99-105, https://doi.org/10.5806/AST.2013.26.1.099
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Abstract
염모제품 중 유효성분의 품질검사는 식품의약품안전청의「의약외품에 관한 기준 및 시험방법」에 따라 제품에 표기된 산화염료들을 박층크로마토그래프법(TLC방법)으로 확인시험을 하도록 되어있다. 그러나 TLC방법은 원료분량이 미량이거나, Rf 값이 비슷한 성분들이 존재하면 확인시험이 어려운 문제점이 있다. 본 연구에서는 미량성분 검출이 용이하며 분석시간이 짧다고 보고된 UPLC를 이용하기 위한시료 전처리 및 분석조건을 탐색하였다. 유효성분들을 분석할 수 있는 검출한계는 6.7-77.9 μg/L, 정량한계는 22.3-259.7 μg/L 이었으며, 회수율은 α-naphthol를 제외하고는 96.2-101.5%로 양호하였다. 유효성분 추출하기 위한 시료 전처리에는 헥산-증류수를 사용하였다. 시료 전처리 시 복잡한 추출과정을 거치지 않고, UPLC방법은 빠르고 정확하게 염모제품에 함유되어 있는 유효성분들을 동시에 분석 할 수 있었다.
- keywords
- oxidative hair dyes, hair coloring products, quality inspection, TLC, UPLC
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